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Synthesis and cytotoxic activity of some (+)-salsolidine derivatives.
Koval'skaya A, Gil'mutdinov A, Lobov A, Tsypyshev D, Vakhitov V, Tsypysheva I, Dokichev V, Vakhitova Y. Koval'skaya A, et al. Nat Prod Res. 2023 Oct 24:1-6. doi: 10.1080/14786419.2023.2273924. Online ahead of print. Nat Prod Res. 2023. PMID: 37874662
On the basis of typical for secondary amino group reactions a number of derivatives of alkaloid (+)-salsolidine was synthesised. Cytotoxic properties of obtained compounds towards the HEK293, A549, MCF-7 and SH-SY5Y cell lines have been evaluated. ...
On the basis of typical for secondary amino group reactions a number of derivatives of alkaloid (+)-salsolidine was synthesised. Cyto …
Breaking Symmetry: Engineering Single-Chain Dimeric Streptavidin as Host for Artificial Metalloenzymes.
Wu S, Zhou Y, Rebelein JG, Kuhn M, Mallin H, Zhao J, Igareta NV, Ward TR. Wu S, et al. J Am Chem Soc. 2019 Oct 9;141(40):15869-15878. doi: 10.1021/jacs.9b06923. Epub 2019 Sep 25. J Am Chem Soc. 2019. PMID: 31509711 Free PMC article.
The practicality of scdSav-based ArMs was illustrated for the reduction of the salsolidine precursor (500 mM) to afford (R)-salsolidine in 90% ee and >17 000 TONs. ...
The practicality of scdSav-based ArMs was illustrated for the reduction of the salsolidine precursor (500 mM) to afford (R)-salsol …
Synthesis of 1-substituted tetrahydroisoquinolines by lithiation and electrophilic quenching guided by in situ IR and NMR spectroscopy and application to the synthesis of salsolidine, carnegine and laudanosine.
Li X, Leonori D, Sheikh NS, Coldham I. Li X, et al. Chemistry. 2013 Jun 10;19(24):7724-30. doi: 10.1002/chem.201301096. Epub 2013 May 15. Chemistry. 2013. PMID: 23677770
The chemistry was applied to N-Boc-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline and led to the efficient synthesis of the racemic alkaloids salsolidine, carnegine, norlaudanosine and laudanosine....
The chemistry was applied to N-Boc-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline and led to the efficient synthesis of the racemic alkaloids …
Spectrophotometric assay of salsolidine hydrochloride.
Karawya MS, Diab AM. Karawya MS, et al. J Assoc Off Anal Chem. 1975 Nov;58(6):1169-70. J Assoc Off Anal Chem. 1975. PMID: 1194179
The proposed method is based on the reaction of salsolidine HCl with carbon disulfide and ammoniacal copper sulfate. ...The method is applicable for the detection of 40-500 mug salsolidine/5 ml....
The proposed method is based on the reaction of salsolidine HCl with carbon disulfide and ammoniacal copper sulfate. ...The method is …
Demonstration of highly specific and sensitive antibodies to a naturally occurring tetrahydroisoquinoline alkaloid, salsolidine.
Stammel W, Müller R, Thomas H. Stammel W, et al. Int J Biochem. 1993 Jun;25(6):917-27. doi: 10.1016/0020-711x(93)90248-d. Int J Biochem. 1993. PMID: 8344447
By immunization of rabbits with salsolidine-BSA conjugate antisalsolidine antibodies were produced. 4. At a final dilution of 1:1700 the highest-titre antiserum bound 35% of 0.21 pmol [3H]salsolidine. This antiserum was used to develop a radioimmunoassay for sals …
By immunization of rabbits with salsolidine-BSA conjugate antisalsolidine antibodies were produced. 4. At a final dilution of 1:1700 …
Stereospecific N-methylation of the tetrahydroisoquinoline alkaloids isosalsoline and salsolidine by amine N-methyltransferase A from bovine liver.
Bahnmaier AH, Woesle B, Thomas H. Bahnmaier AH, et al. Chirality. 1999;11(2):160-5. doi: 10.1002/(SICI)1520-636X(1999)11:2<160::AID-CHIR13>3.0.CO;2-M. Chirality. 1999. PMID: 9951405
Stereospecific N-methylation of the tetrahydroisoquinoline alkaloids isosalsoline (7-hydroxy-6-methoxy-1-methyl-1,2,3,4-tetrahydroisoquinoline) and salsolidine (6,7-dimethoxy-1-methyl-1,2,3,4-tetrahydroisoquinoline) by amine N-methyltransferase A isolated from bovine liver …
Stereospecific N-methylation of the tetrahydroisoquinoline alkaloids isosalsoline (7-hydroxy-6-methoxy-1-methyl-1,2,3,4-tetrahydroisoquinoli …
Structural, kinetic, and docking studies of artificial imine reductases based on biotin-streptavidin technology: an induced lock-and-key hypothesis.
Robles VM, Dürrenberger M, Heinisch T, Lledós A, Schirmer T, Ward TR, Maréchal JD. Robles VM, et al. J Am Chem Soc. 2014 Nov 5;136(44):15676-83. doi: 10.1021/ja508258t. Epub 2014 Oct 28. J Am Chem Soc. 2014. PMID: 25317660
Mutation of S112 reveals a marked effect of the Ir/streptavidin ratio on both the saturation kinetics as well as the enantioselectivity for the production of salsolidine. For [Cp*Ir(Biot-p-L)Cl] S112A Sav, both the reaction rate and the selectivity (up to 96% ee (R)-sal …
Mutation of S112 reveals a marked effect of the Ir/streptavidin ratio on both the saturation kinetics as well as the enantioselectivity for …
Conformational analysis of an isoquinolinium hydrochloride in water using residual dipolar couplings.
Trigo-Mouriño P, Santamaría-Fernández R, Sánchez-Pedregal VM, Navarro-Vázquez A. Trigo-Mouriño P, et al. J Org Chem. 2010 May 7;75(9):3101-4. doi: 10.1021/jo902502h. J Org Chem. 2010. PMID: 20345159
The use of the cetylpyridinium chloride (CPCL)/NaCl/hexanol liquid crystal allowed the measurement of (1)D(CH) residual dipolar couplings of the isoquinoline alkaloid salsolidine in its protonated state. Populations of its two half-chair forms were determined by using the …
The use of the cetylpyridinium chloride (CPCL)/NaCl/hexanol liquid crystal allowed the measurement of (1)D(CH) residual dipolar couplings of …
30 results