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Chiral Discrimination Mechanisms by Silylated-Acetylated Cyclodextrins: Superficial Interactions vs. Inclusion.
Balzano F, Uccello-Barretta G, Sicoli G, Vanni L, Recchimurzo A, Aiello F. Balzano F, et al. Int J Mol Sci. 2022 Oct 29;23(21):13169. doi: 10.3390/ijms232113169. Int J Mol Sci. 2022. PMID: 36361950 Free PMC article.
The purpose of this study is to compare via nuclear magnetic resonance (NMR) spectroscopy the efficiency of silylated-acetylated alpha-, beta-, and gamma-cyclodextrins in the chiral discrimination of 1,1,1,3,3-pentafluoro-2-(fluoromethoxy)-3-methoxypropane (compound B) and met …
The purpose of this study is to compare via nuclear magnetic resonance (NMR) spectroscopy the efficiency of silylated-acetylated alpha-, bet …
Direct determination of the enantiomeric purity or enantiomeric composition of methylpropionates using a single capacitive microsensor.
Kurzawski P, Bogdanski A, Schurig V, Wimmer R, Hierlemann A. Kurzawski P, et al. Anal Chem. 2009 Mar 1;81(5):1969-75. doi: 10.1021/ac802455c. Anal Chem. 2009. PMID: 19191479
Capacitive enantioselective sensors have been demonstrated to provide antipodal signals upon dosage of, e.g., the enantiomers of methyl lactate or methyl-2-chloropropionate. In a next step, these sensors have been used to not only qualitatively determine the …
Capacitive enantioselective sensors have been demonstrated to provide antipodal signals upon dosage of, e.g., the enantiomers of methyl lact …
Highly-reactive haloester surface initiators for ARGET ATRP readily prepared by radio frequency glow discharge plasma.
Mecwan MM, Taylor MJ, Graham DJ, Ratner BD. Mecwan MM, et al. Biointerphases. 2019 Aug 22;14(4):041006. doi: 10.1116/1.5110163. Biointerphases. 2019. PMID: 31438685 Free PMC article.
New surface initiators for ARGET ATRP (activators regenerated by electron transfer atomic transfer radical polymerization) have been prepared by the plasma deposition of haloester monomers. Specifically, methyl 3-bromopropionate (M3BP), methyl 2-chloropropionate …
New surface initiators for ARGET ATRP (activators regenerated by electron transfer atomic transfer radical polymerization) have been prepare …
Stereoblock copolymers and tacticity control in controlled/living radical polymerization.
Lutz JF, Neugebauer D, Matyjaszewski K. Lutz JF, et al. J Am Chem Soc. 2003 Jun 11;125(23):6986-93. doi: 10.1021/ja029517w. J Am Chem Soc. 2003. PMID: 12783552

Poly(N,N-dimethylacrylamide) with controlled molecular weight, low polydispersity (M(w)/M(n) < 1.2), and a high proportion of meso dyads ( approximately 85%) was prepared by ATRP (with initiating system methyl 2-chloropropionate/CuCl/Me(6)TREN) and RAFT (w

…

Poly(N,N-dimethylacrylamide) with controlled molecular weight, low polydispersity (M(w)/M(n) < 1.2), and a high proportion of meso dyads

…
Chiral sensing using a complementary metal-oxide semiconductor-integrated three-transducer microsensor system.
Kurzawski P, Schurig V, Hierlemann A. Kurzawski P, et al. Anal Chem. 2009 Nov 15;81(22):9353-64. doi: 10.1021/ac9017007. Anal Chem. 2009. PMID: 19842695
Upon exposure to chiral analytes, such as methyl lactate and methyl-2-chloropropionate, all three transducers showed distinct chiral discrimination of these analytes. ...
Upon exposure to chiral analytes, such as methyl lactate and methyl-2-chloropropionate, all three transducers showed di …
Chiral discrimination of inhalation anesthetics and methyl propionates by thickness shear mode resonators: new insights into the mechanisms of enantioselectivity by cyclodextrins.
Bodenhöfer K, Hierlemann A, Juza M, Schurig V, Göpel W. Bodenhöfer K, et al. Anal Chem. 1997 Oct 1;69(19):4017-31. doi: 10.1021/ac970367v. Anal Chem. 1997. PMID: 9322439
The discrimination of the enantiomers of methyl lactate, methyl 2-chloropropionate, and the inhalation anesthetics enflurane, isoflurane, and desflurane in the gas phase has been performed using thickness shear mode resonators. ...
The discrimination of the enantiomers of methyl lactate, methyl 2-chloropropionate, and the inhalation anesthetics enfl …
Synergistic effects of trace amounts of water in the enantiodiscrimination processes by lipodex E: a spectroscopic and computational investigation.
Uccello-Barretta G, Schurig V, Balzano F, Vanni L, Aiello F, Mori M, Ghirga F. Uccello-Barretta G, et al. Chirality. 2015 Feb;27(2):95-103. doi: 10.1002/chir.22394. Epub 2014 Oct 20. Chirality. 2015. PMID: 25330235
Nuclear magnetic resonance (NMR) investigations on mixtures containing octakis(3-O-butanoyl-2,6-di-O-pentyl)-gamma-cyclodextrin (Lipodex E) and each enantiomer of methyl-2-chloropropionate (MCP) ascertained the role of trace amounts of water in the enantiodis …
Nuclear magnetic resonance (NMR) investigations on mixtures containing octakis(3-O-butanoyl-2,6-di-O-pentyl)-gamma-cyclodextrin (Lipodex E) …
14 results