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Formation of methyl ester of 2-methylglyceric acid from thymine glycol residues: a convenient new method for determining radiation damage to DNA.
Schellenberg KA, Shaeffer J. Schellenberg KA, et al. Biochemistry. 1986 Apr 8;25(7):1479-82. doi: 10.1021/bi00355a002. Biochemistry. 1986. PMID: 3707888
Thymine glycol residues in DNA or thymidine were converted to methyl 2-methylglycerate by reaction with alkaline borohydride followed by methanolic HCl. ...The data indicate that certain oxidants including hydroxyl radicals generated by chemical means or from …
Thymine glycol residues in DNA or thymidine were converted to methyl 2-methylglycerate by reaction with alkaline borohy …
Gas chromatographic-mass spectrometric method for the assessment of oxidative damage to double-stranded dna by quantification of thymine glycol residues.
Markey SP, Markey CJ, Wang TC, Rodriguez JB. Markey SP, et al. J Am Soc Mass Spectrom. 1993 Apr;4(4):336-42. doi: 10.1016/1044-0305(93)85056-4. J Am Soc Mass Spectrom. 1993. PMID: 24234868
The procedure utilizes base to ring-open DNA-bound thymine glycol in the presence of monomeric [(2)H4]thymine glycol as an internal standard, followed by reduction, solvolytic cleavage, and quantification of the characteristic methyl-2-methylglycerate release …
The procedure utilizes base to ring-open DNA-bound thymine glycol in the presence of monomeric [(2)H4]thymine glycol as an internal standard …
Characterization of anthraquinone-2-carbonyl chloride as an alcohol derivatization reagent for negative ion chemical ionization mass spectrometry.
Simpson JT, Torok DS, Worman R, Quearry BJ, Markey SP, Ziffer H. Simpson JT, et al. J Am Soc Mass Spectrom. 1995 Feb;6(2):148-51. doi: 10.1016/S1044-0305(94)00107-B. J Am Soc Mass Spectrom. 1995. PMID: 24222077
A series of model compounds, 2-phenylethanol (phenethyl alcohol), 1-phenyl-2-propanol, 2-methyl-l-phenyl-2-propanol, hexanol, and methyl 2-methylglycerate, were used as analytes.The particle beam LC/MS properties of the resultant anthraquinone carboxylate est …
A series of model compounds, 2-phenylethanol (phenethyl alcohol), 1-phenyl-2-propanol, 2-methyl-l-phenyl-2-propanol, hexanol, and methyl