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2,2'-Ethylenebis(1,3-dithiane) as a polydentate mu(2)-, mu(4)- and mu(5)-assembling ligand for the construction of sulphur-rich Cu(I), Hg(II) and heterometallic Cu(I)/Hg(II) coordination polymers featuring uncommon network architectures.
Viau L, Knorr M, Knauer L, Brieger L, Strohmann C. Viau L, et al. Dalton Trans. 2022 May 17;51(19):7581-7606. doi: 10.1039/d2dt00800a. Dalton Trans. 2022. PMID: 35507431
In the case of HgBr(2), using a 2 : 1 metal-to-ligand ratio, 1D polymeric [{BrHg(mu(2)-Br)(2)HgBr}(mu(2)-L1)] (CP10) is produced. HgI(2) and HgBr(2) have also been reacted with 2-methyl-1,3-dithiane L2 yielding the molecular complexes [{IHg(mu(2 …
In the case of HgBr(2), using a 2 : 1 metal-to-ligand ratio, 1D polymeric [{BrHg(mu(2)-Br)(2)HgBr}(mu(2)-L1)] (CP10) is produced. HgI(2) and …
1,3-Dithianes as Assembling Ligands for the Construction of Copper(I) Coordination Polymers. Investigation of the Impact of the RC(H)S2C3H6 Substituent and Reaction Conditions on the Architecture of the 0D-3D Networks.
Raghuvanshi A, Knorr M, Knauer L, Strohmann C, Boullanger S, Moutarlier V, Viau L. Raghuvanshi A, et al. Inorg Chem. 2019 May 6;58(9):5753-5775. doi: 10.1021/acs.inorgchem.9b00114. Epub 2019 Apr 23. Inorg Chem. 2019. PMID: 31013066
The 1D compounds [{Cu(mu(2)-X)(2)Cu}(mu(2)-L2)(2)] (n) (CP7, X = Br, and CP8, X = Cl) resulting from treatment of 2-methyl-1,3 dithiane (L2) with CuBr and CuCl are isostructural with their CuI homologue [{Cu(mu(2)-I)(2)Cu}(mu(2)-L2)(2)] (n) (CP5 …
The 1D compounds [{Cu(mu(2)-X)(2)Cu}(mu(2)-L2)(2)] (n) (CP7, X = Br, and CP8, X = Cl) resulting from treatment of 2-methyl- …
5-tert-Butyl-2-(4'-[18F]fluoropropynylphenyl)-1,3-dithiane oxides: potential new GABA A receptor radioligands.
Li X, Jung YW, Snyder SE, Blair J, Sherman PS, Desmond T, Frey KA, Kilbourn MR. Li X, et al. Nucl Med Biol. 2008 Jul;35(5):549-59. doi: 10.1016/j.nucmedbio.2007.08.003. Epub 2007 Nov 26. Nucl Med Biol. 2008. PMID: 18589299 Free PMC article.
As potential new ligands targeting the binding site of gamma-aminobutyric acid (GABA) receptor ionophore, trans-5-tert-butyl-2-(4'-fluoropropynylphenyl)-2-methyl-1,1-dioxo-1,3-dithiane (1) and cis/trans-5-tert-butyl-2-(4'-fluoropropynylphenyl)- …
As potential new ligands targeting the binding site of gamma-aminobutyric acid (GABA) receptor ionophore, trans-5-tert-butyl-2-(4'-fluoropro …
Synthesis of carbon-11-, fluorine-18-, and iodine-125-labeled GABAA-gated chloride ion channel blockers: substituted 5-tert-butyl-2-phenyl-1,3-dithianes and -dithiane oxides.
Snyder SE, Kume A, Jung YW, Connor SE, Sherman PS, Albin RL, Wieland DM, Kilbourn MR. Snyder SE, et al. J Med Chem. 1995 Jul 7;38(14):2663-71. doi: 10.1021/jm00014a018. J Med Chem. 1995. PMID: 7629805
Of the eight compounds tested, trans-5-tert-butyl-2-(4-cyanophenyl)-2-methyl-1,1,3,3-tetraoxo+ ++-1,3-dithiane, 9b, trans-5-tert-butyl-2-(4-fluorophenyl)-1,1,3,3-tetraoxo-1,3-dithian e, 10, and trans-5-tert-butyl-2-(4-iodophenyl)-2-met …
Of the eight compounds tested, trans-5-tert-butyl-2-(4-cyanophenyl)-2-methyl-1,1,3,3-tetraoxo+ ++-1,3-dithian …
Elucidating heteroatom influence on homonuclear 4 J(H,H) coupling constants by DFT/NMR approach.
Chini MG, Urbani D, Dambruoso P, Riccio R, Bifulco G. Chini MG, et al. Magn Reson Chem. 2020 Jun;58(6):566-575. doi: 10.1002/mrc.4983. Epub 2020 Jan 24. Magn Reson Chem. 2020. PMID: 31883165
The (4) J((H,H)) calculated values, tabulated for variation of 30 for both phi1 and phi3, have disclosed an unexpected detectable coupling constant ((4) J((H,H) ) 1 Hz) across heteroatoms, useful to provide valuable structural information. A 2-methyl-1,3 …
The (4) J((H,H)) calculated values, tabulated for variation of 30 for both phi1 and phi3, have disclosed an unexpected detectable coupling c …
The role of hyperconjugation in the conformational analysis of methylcyclohexane and methylheterocyclohexanes.
Ribeiro DS, Rittner R. Ribeiro DS, et al. J Org Chem. 2003 Aug 22;68(17):6780-7. doi: 10.1021/jo034421l. J Org Chem. 2003. PMID: 12919048
Full geometry optimizations were carried out at the HF/6-31G** and B3LYP/6-31G** levels for methylcyclohexane, 2-, 3-, and 4-methyltetrahydropyran, 2-, 3-, and 4-methylpiperidine, 2-, 3-, and 4-methylthiane, 2-, 4-, and 5-methyl-1,3-dioxane, and 2-, 4-, and 5-methyl-1,3- …
Full geometry optimizations were carried out at the HF/6-31G** and B3LYP/6-31G** levels for methylcyclohexane, 2-, 3-, and 4-methyltetrahydr …
Ring-expansion of thioacetal ring via bicyclosulfonium ylide. Effect Of protic nucleophile on ylide intermediate.
Mori T, Sawada Y, Oku A. Mori T, et al. J Org Chem. 2000 Jun 16;65(12):3620-5. doi: 10.1021/jo991775x. J Org Chem. 2000. PMID: 10864744
The reaction of 2-(3-diazo-2-oxopropane-1-yl)-2-methyldithiolane 9a, 2-(4-diazo-3-oxobutane-2-yl)-2-methyldithiolane 9c, and 2-(3-diazo-2-oxopropane-1-yl)-2-methyl-1,3-dithiane 9b with Rh(2)(OAc)(4) gave three-carbon ring-expansion products dith …
The reaction of 2-(3-diazo-2-oxopropane-1-yl)-2-methyldithiolane 9a, 2-(4-diazo-3-oxobutane-2-yl)-2-methyldithiolane 9c, and 2-(3-diazo-2-ox …
Distonic ion .CH2CH2SCH2+ and the isomeric trimethylene and propylene sulfide radical cations. Assessment of structures and reactivities via decomposition and redox reactions.
Polce MJ, Wesdemiotis C. Polce MJ, et al. Rapid Commun Mass Spectrom. 1996;10(2):235-41. doi: 10.1002/(SICI)1097-0231(19960131)10:2<235::AID-RCM472>3.0.CO;2-1. Rapid Commun Mass Spectrom. 1996. PMID: 8616267
The dissociations and redox reactions of the propylene sulfide ion (3+.) are also assessed in this study and clearly indicate that 3+. is a stable C3H6S+. isomer. Further, the C3H6S+. ions from thiane, 1,3-dithiane and 2-methyl-1,3-dit …
The dissociations and redox reactions of the propylene sulfide ion (3+.) are also assessed in this study and clearly indicate that 3+. is a …
Control of Structures and Emission Properties of (CuI) n 2-Methyldithiane Coordination Polymers.
Schlachter A, Viau L, Fortin D, Knauer L, Strohmann C, Knorr M, Harvey PD. Schlachter A, et al. Inorg Chem. 2018 Nov 5;57(21):13564-13576. doi: 10.1021/acs.inorgchem.8b02168. Epub 2018 Oct 22. Inorg Chem. 2018. PMID: 30346744
A structurally unique and strongly luminescent nonporous 3D coordination polymer (CP) [Cu(8)I(8)(methyldithiane)(4)] (n), CP3, has been prepared in a quasi-anticipated manner from 2-methyl-1,3-dithiane, L1, and CuI. This CP incorporates an unpre …
A structurally unique and strongly luminescent nonporous 3D coordination polymer (CP) [Cu(8)I(8)(methyldithiane)(4)] (n), CP3, has been prep …
Enhanced efficacy of combinations of retinoic acid- and retinoid X receptor-selective retinoids and alpha-interferon in inhibition of cervical carcinoma cell proliferation.
Lotan R, Dawson MI, Zou CC, Jong L, Lotan D, Zou CP. Lotan R, et al. Cancer Res. 1995 Jan 15;55(2):232-6. Cancer Res. 1995. PMID: 7812950
In contrast, two other retinoids [2-(4-carboxyphenyl)-2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2- naphthalenyl)-1,3-dithiane (SR11203) and 4-(2-methyl-1-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2- naphthalenyl)propenyl)benzoic acid (SR11217)], w …
In contrast, two other retinoids [2-(4-carboxyphenyl)-2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2- naphthalenyl)-1,3-dithiane …
12 results