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27526091,24097402,28081498,25125396,28372841,28864231,30476592,24861873,27993879,34013677,26451531,23239334,26171884,31715032,33091679,24670084,26536779,21245371,34721288,28622619,34432104,25967149,20136128,20381436,24576767,16020493,23050454,27656337,23123828,30403208,27180887,31958632,27112381,33819798,24714680,24828488,28917261,26708628,30611909,26054580,27614352,27240300,21328697,21248072,32592276,28842174,25168117,18087693,26874878,24473373,18279671,33259939,34500616,29486367,34435207,30205156,21907190,22265352,33352934,37131118,19389886,21601563,36336861,26513621,19850018,35572785,11456110,34463312,30553931,21569549,25955382,34913542,26388380,21171171,26120794,31199458,28153274,27052537,8392394,16690491,28433267,25195024,26718874,36705732,23001980,26931428,26602143,36107130,28193495,32890769,36127620,26690787,26602141,34727586,1443523,31334481,26924585,36371780,26864540,23386645,30541089,29863032,22771503,28138745,31592654,1655127,35458625,30231011,16574756,30912169,27863211,21768219,20046660,30292631,9816377,28741469,25710460,19842995,24749986,25291951,31715316,20399267,29432962,28304097,21047880,15859623,9226581,26609169,6972726,29229333,32529210,26441239,3501463,26713090,25868511,36806449,26124054,31443425,28506446,30015370,34010687,25833687,18325178,28242262,36692589,28403556,8516267,23811497,35931233,27570062,34719610,27595769,6333810,25545356,33352890,27468563,36342509,9174267,25183657,31060022,33167291,28492140,31352023,1329183,33662569,21784054,32592191,24423328,6603929,31875826,36404469,35503795,2600668,27208559,34632483,24885631,35934272,31071583,12834240,26684022,6974771,34836390,24486315,34184102,28315849,3877975,33636208,25845705,36750341,27282116,32270886,30710745,26359234,30471219,28199350,2783695,36982565,23831447,26585929,20206693,22244986,27257343,33780622,9300907,27896775,2551121,35659347,28863788,29172936,26272200,26302850,2556781,30476591,30987722,28375002,27715010,29217650,29534611,20881084,24703961,22968104,30713278,32841780,22536763,28148721,18437365,34774725,35849629,25402376,32302333,35514251,35768249,33174880,28116494,28437713,35501505,26772722,12093529,6280344,34954017,35031430,3500819,6966982,22533908,26110032,6974620,33109163,10430245,24645519,18927245,34394078,35220442,30761082,34201027,3153059,29633224,3003603,33516786,24830152,8180121,26457778,9366501,18957567,27522099,24476080,7951544,23852785,26548417,24000372,28822224,31352025,29295513,6982126,6604797,25601703,28182348,25578393,32751196,32928351,6250743,33856702,1867383,35684001,28501210,32533980,31428669,35138814,3024685,3039769,11393696,2271359,22925701,23978484,1369418,20628873,34750644,27741217,11762789,6329553,26655254,31639671,1337903,28847346,30088075,32693895,23539484,34572501,24045553,6546303,30633541,28801845,36127619,33184642,22816247,31415098,10443483,31417914,26594646,18801940,27540205,29476721,20795940,30537386,27633775,35487016,30876571,2783577,21983164,29053944,30692037,36374723,36191978,32649998,16339300,31851610,8124861,33722092,34836003,29709871,7628077,9838212,34606802,2853987,6411087,33199793,33062234,25922442,25462357,6608135,32241530,34164449,29479885,31573878,26220765,26865648,35911100,3840418,35337847,35904704,33713691,23377091,34418538,6974772,31787743,30115398,34570174,35654380,24152903,6974062,27045951,3494111,33933982,9518141,33825696,6286379,31804956,33269020,31550504,6335776,19103962,12007767,35908594,25145136,22816246,29886288,31832707,10704005,29935177,6969637,31095673,33876919,30654110,33365128,32432371,36870118,22536761,2835464,26093339,32684140,34282678,18095078,20188118,17548449,22515958,8408412,30530114,2253400,31260261,6611226,35561028,2339276,25004404,36625245,2585144,29652819,35764669,25258283,31988650,2850225,31193444,36688810,23555079,6488566,34444934,25132191,32704612,20493831,35703250,36557317,30248720,34909515,17955977,22808099,2243289,34836187,34950834,22632164,1535819,29920712,21391498,33119540,33491437,28822355,7586974,34285353,28975688,10605895,7577703,34206219,1332539,36639845,2543519,23695296,25045351,28988826,23025817,29729124,35238975,27005269,29792047,35326710,9191544,2397607,9749834,3877663,35779863,29726119,30026263,9106025,19779960,7510592,19042996,35626384,30775503,3085890,33255807,6602540,7846739,33775819,25434745,3841227,23210651,657481,28842822,36279170,1959339,29166995,36977791,31452227,25403087,28786376,6607788,26445902,9827027,35498132,25107951,29955644,22155920,30868850,29329431,8605676,21914787,22536762,29597233,26130585,23525585,35893730,28169461,36830861,16751686,33636826,17077543,24217904,21896243,28623654,36785905,33443406,8897577,35368147,24343452,24821067,7748191,36103653,6719023,29852126,34687521,34419456,34455342,35874521,6982954,24714142,8410371,32802551,22848531,6677649,3873464,32942601,36570156,23814673,30292290,33847203,31940808,22211693,10751640,25053051,1667458,8424897,36109397,32052638,30475076,25905750,32311429,15609867,3180464,24094638,33241273,28335977,8939776,37111224,32496995,35982251,31330127,32550812,9106064,34556212,24721864,65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691 results

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Development and validation of the simultaneous measurement of four vitamin D metabolites in serum by LC-MS/MS for clinical laboratory applications.

Satoh M, Ishige T, Ogawa S, Nishimura M, Matsushita K, Higashi T, Nomura F. Satoh M, et al. Anal Bioanal Chem. 2016 Nov;408(27):7617-7627. doi: 10.1007/s00216-016-9821-4. Epub 2016 Aug 15. Anal Bioanal Chem. 2016. PMID: 27526091

A novel Cookson-type reagent for enhancing sensitivity and specificity in assessment of infant vitamin D status using liquid chromatography/tandem mass spectrometry.

Ogawa S, Ooki S, Morohashi M, Yamagata K, Higashi T. Ogawa S, et al. Rapid Commun Mass Spectrom. 2013 Nov 15;27(21):2453-60. doi: 10.1002/rcm.6708. Rapid Commun Mass Spectrom. 2013. PMID: 24097402

Enhancing analysis throughput, sensitivity and specificity in LC/ESI-MS/MS assay of plasma 25-hydroxyvitamin D₃ by derivatization with triplex 4-(4-dimethylaminophenyl)-1,2,4-triazoline-3,5-dione (DAPTAD) isotopologues.

Ogawa S, Kittaka H, Nakata A, Komatsu K, Sugiura T, Satoh M, Nomura F, Higashi T. Ogawa S, et al. J Pharm Biomed Anal. 2017 Mar 20;136:126-133. doi: 10.1016/j.jpba.2016.11.030. Epub 2016 Nov 17. J Pharm Biomed Anal. 2017. PMID: 28081498

Overestimation of 25-hydroxyvitamin D3 by increased ionisation efficiency of 3-epi-25-hydroxyvitamin D3 in LC-MS/MS methods not separating both metabolites as determined by an LC-MS/MS method for separate quantification of 25-hydroxyvitamin D3, 3-epi-25-hydroxyvitamin D3 and 25-hydroxyvitamin D2 in human serum.

van den Ouweland JM, Beijers AM, van Daal H. van den Ouweland JM, et al. J Chromatogr B Analyt Technol Biomed Life Sci. 2014 Sep 15;967:195-202. doi: 10.1016/j.jchromb.2014.07.021. Epub 2014 Jul 31. J Chromatogr B Analyt Technol Biomed Life Sci. 2014. PMID: 25125396

Improved accuracy of an tandem liquid chromatography-mass spectrometry method measuring 24R,25-dihydroxyvitamin D₃ and 25-hydroxyvitamin D metabolites in serum using unspiked controls and its application to determining cross-reactivity of a chemiluminescent microparticle immunoassay.

Dowling KG, Hull G, Sundvall J, Lamberg-Allardt C, Cashman KD. Dowling KG, et al. J Chromatogr A. 2017 May 12;1497:102-109. doi: 10.1016/j.chroma.2017.03.058. Epub 2017 Mar 23. J Chromatogr A. 2017. PMID: 28372841

Improved sensitivity of serum/plasma 1α,25-dihydroxyvitamin D quantification by DAPTAD derivatization.

Ishige T, Satoh M, Ogawa S, Nishimura M, Matsushita K, Higashi T, Nomura F. Ishige T, et al. Clin Chim Acta. 2017 Oct;473:173-179. doi: 10.1016/j.cca.2017.08.033. Epub 2017 Aug 31. Clin Chim Acta. 2017. PMID: 28864231

Rapid liquid chromatography-tandem mass spectrometry method for determination of 24,25(OH)₂D and 25OHD with efficient separation of 3-epi analogs.

Yu S, Zhou W, Wang D, Yin Y, Cheng Q, Xie S, Sun D, Li H, Cheng X, Qiu L. Yu S, et al. J Steroid Biochem Mol Biol. 2019 Mar;187:146-151. doi: 10.1016/j.jsbmb.2018.11.012. Epub 2018 Nov 23. J Steroid Biochem Mol Biol. 2019. PMID: 30476592

Development and validation of an LC-MS/MS based method for quantification of 25 hydroxyvitamin D2 and 25 hydroxyvitamin D3 in human serum and plasma.

Zhang SW, Jian W, Sullivan S, Sankaran B, Edom RW, Weng N, Sharkey D. Zhang SW, et al. J Chromatogr B Analyt Technol Biomed Life Sci. 2014 Jun 15;961:62-70. doi: 10.1016/j.jchromb.2014.05.006. Epub 2014 May 14. J Chromatogr B Analyt Technol Biomed Life Sci. 2014. PMID: 24861873

A Rapid and Simple Liquid-Chromatography-Tandem Mass Spectrometry Method for Measuring 25-Hydroxyvitamin D2 and 25-Hydroxyvitamin D3 in Human Serum: Comparison with Two Automated Immunoassays.

Lee S, Kim JH, Kim SA, Sun YS, Lee A, Park SJ, Kim YT, Lee KR, Kim YJ. Lee S, et al. Ann Clin Lab Sci. 2016 Dec;46(6):645-653. Ann Clin Lab Sci. 2016. PMID: 27993879

Simultaneous measurement of 13 circulating vitamin D3 and D2 mono and dihydroxy metabolites using liquid chromatography mass spectrometry.

Jenkinson C, Desai R, Slominski AT, Tuckey RC, Hewison M, Handelsman DJ. Jenkinson C, et al. Clin Chem Lab Med. 2021 May 20;59(10):1642-1652. doi: 10.1515/cclm-2021-0441. Print 2021 Sep 27. Clin Chem Lab Med. 2021. PMID: 34013677 Free PMC article.

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