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Items: 1 to 50 of 90

1.

Structural properties of D-mannopyranosyl rings containing O-acetyl side-chains.

Turney T, Zhang W, Oliver AG, Serianni AS.

Acta Crystallogr C Struct Chem. 2019 Aug 1;75(Pt 8):1166-1174. doi: 10.1107/S2053229619008817. Epub 2019 Jul 29.

PMID:
31380800
2.

Conformational analysis of the disaccharide methyl α-D-mannopyranosyl-(1→3)-2-O-acetyl-β-D-mannopyranoside monohydrate.

Zhang W, Wu Q, Oliver AG, Serianni AS.

Acta Crystallogr C Struct Chem. 2019 Jun 1;75(Pt 6):610-615. doi: 10.1107/S2053229619004728. Epub 2019 May 14.

PMID:
31166911
3.

O-Benzoyl side-chain conformations in 2,3,4,6-tetra-O-benzoyl-β-D-galactopyranosyl-(1→4)-1,2,6-tri-O-benzoyl-β-D-glucopyranose (ethyl acetate solvate) and 1,2,4,6-tetra-O-benzoyl-β-D-glucopyranose (acetone solvate).

Turney T, Pan Q, Zhang W, Oliver AG, Serianni AS.

Acta Crystallogr C Struct Chem. 2019 Feb 1;75(Pt 2):161-167. doi: 10.1107/S2053229619000822. Epub 2019 Jan 25.

PMID:
30720454
4.

Synthesis and O-Glycosidic Linkage Conformational Analysis of 13C-Labeled Oligosaccharide Fragments of an Antifreeze Glycolipid.

Zhang W, Meredith R, Yoon MK, Wang X, Woods RJ, Carmichael I, Serianni AS.

J Org Chem. 2019 Feb 15;84(4):1706-1724. doi: 10.1021/acs.joc.8b01411. Epub 2019 Jan 29.

PMID:
30624062
5.

Use of Circular Statistics To Model αMan-(1→2)-αMan and αMan-(1→3)-α/βMan O-Glycosidic Linkage Conformation in 13C-Labeled Disaccharides and High-Mannose Oligosaccharides.

Zhang W, Meredith R, Pan Q, Wang X, Woods RJ, Carmichael I, Serianni AS.

Biochemistry. 2019 Feb 12;58(6):546-560. doi: 10.1021/acs.biochem.8b01050. Epub 2019 Jan 24.

PMID:
30605318
6.

Synthesis of high-mannose oligosaccharides containing mannose-6-phosphate residues using regioselective glycosylation.

Meng B, Wang J, Wang Q, Serianni AS, Pan Q.

Carbohydr Res. 2018 Sep;467:23-32. doi: 10.1016/j.carres.2018.07.005. Epub 2018 Jul 31.

PMID:
30075362
7.

Rapid assembly of branched mannose oligosaccharides through consecutive regioselective glycosylation: A convergent and efficient strategy.

Meng B, Wang J, Wang Q, Serianni AS, Pan Q.

Tetrahedron. 2017 Jul 6;73(27-28):3932-3938. doi: 10.1016/j.tet.2017.05.073. Epub 2017 May 22.

8.

Enzymatic synthesis of ribo- and 2'-deoxyribonucleosides from glycofuranosyl phosphates: An approach to facilitate isotopic labeling.

Zhang W, Turney T, Surjancev I, Serianni AS.

Carbohydr Res. 2017 Sep 8;449:125-133. doi: 10.1016/j.carres.2017.07.006. Epub 2017 Jul 20.

PMID:
28780317
9.

Conformational Populations of β-(1→4) O-Glycosidic Linkages Using Redundant NMR J-Couplings and Circular Statistics.

Zhang W, Turney T, Meredith R, Pan Q, Sernau L, Wang X, Hu X, Woods RJ, Carmichael I, Serianni AS.

J Phys Chem B. 2017 Apr 13;121(14):3042-3058. doi: 10.1021/acs.jpcb.7b02252. Epub 2017 Mar 30.

10.

13C-Labeled Idohexopyranosyl Rings: Effects of Methyl Glycosidation and C6 Oxidation on Ring Conformational Equilibria.

Bose-Basu B, Zhang W, Kennedy JL, Hadad MJ, Carmichael I, Serianni AS.

J Org Chem. 2017 Feb 3;82(3):1356-1370. doi: 10.1021/acs.joc.6b02399. Epub 2017 Jan 24.

PMID:
28006104
11.

O-Acetyl Side-Chains in Monosaccharides: Redundant NMR Spin-Couplings and Statistical Models for Acetate Ester Conformational Analysis.

Turney T, Pan Q, Sernau L, Carmichael I, Zhang W, Wang X, Woods RJ, Serianni AS.

J Phys Chem B. 2017 Jan 12;121(1):66-77. doi: 10.1021/acs.jpcb.6b10028. Epub 2016 Dec 21.

12.

A chemical synthesis of a multiply 13 C-labeled hexasaccharide: a high-mannose N-glycan fragment.

Zhang W, Pan Q, Serianni AS.

J Labelled Comp Radiopharm. 2016 Dec;59(14):673-679. doi: 10.1002/jlcr.3418. Epub 2016 Jul 8.

13.

Labeling monosaccharides with stable isotopes.

Zhang W, Zhao S, Serianni AS.

Methods Enzymol. 2015;565:423-58. doi: 10.1016/bs.mie.2015.06.016. Epub 2015 Aug 6.

PMID:
26577741
14.

Informing saccharide structural NMR studies with density functional theory calculations.

Klepach T, Zhao H, Hu X, Zhang W, Stenutz R, Hadad MJ, Carmichael I, Serianni AS.

Methods Mol Biol. 2015;1273:289-331. doi: 10.1007/978-1-4939-2343-4_20.

PMID:
25753718
15.

Wood frog adaptations to overwintering in Alaska: new limits to freezing tolerance.

Larson DJ, Middle L, Vu H, Zhang W, Serianni AS, Duman J, Barnes BM.

J Exp Biol. 2014 Jun 15;217(Pt 12):2193-200. doi: 10.1242/jeb.101931. Epub 2014 Apr 15.

16.

Methyl 4-O-β-D-xylopyranosyl β-D-mannopyranoside, a core disaccharide of an antifreeze glycolipid.

Zhang W, Oliver AG, Vu HM, Duman JG, Serianni AS.

Acta Crystallogr C. 2013 Sep;69(Pt 9):1047-50. doi: 10.1107/S0108270113019021. Epub 2013 Aug 7.

PMID:
24005519
17.

Methyl 4-O-β-D-mannopyranosyl β-D-xylopyranoside.

Zhang W, Oliver AG, Vu HM, Duman JG, Serianni AS.

Acta Crystallogr C. 2012 Dec;68(Pt 12):o502-6. doi: 10.1107/S0108270112046689. Epub 2012 Nov 29.

PMID:
23221256
18.

Methyl [13C]glucopyranosiduronic acids: effect of COOH ionization and exocyclic structure on NMR spin-couplings.

Zhang W, Hu X, Carmichael I, Serianni AS.

J Org Chem. 2012 Nov 2;77(21):9521-34. doi: 10.1021/jo3011182. Epub 2012 Oct 23.

PMID:
22967209
19.

Phosphate-catalyzed degradation of D-glucosone in aqueous solution is accompanied by C1-C2 transposition.

Zhang W, Serianni AS.

J Am Chem Soc. 2012 Jul 18;134(28):11511-24. doi: 10.1021/ja3020296. Epub 2012 Jul 2.

PMID:
22650268
20.

Dependence of pyranose ring puckering on anomeric configuration: methyl idopyranosides.

Sattelle BM, Bose-Basu B, Tessier M, Woods RJ, Serianni AS, Almond A.

J Phys Chem B. 2012 Jun 7;116(22):6380-6. doi: 10.1021/jp303183y. Epub 2012 May 23.

21.

Disorder and conformational analysis of methyl β-D-galactopyranosyl-(1→4)-β-D-xylopyranoside.

Zhang W, Oliver AG, Serianni AS.

Acta Crystallogr C. 2012 Jan;68(Pt 1):o7-11. doi: 10.1107/S0108270111048347. Epub 2011 Dec 6.

PMID:
22223286
22.

Rearrangement of 3-deoxy-D-erythro-hexos-2-ulose in aqueous solution: NMR evidence of intramolecular 1,2-hydrogen transfer.

Zhang W, Carmichael I, Serianni AS.

J Org Chem. 2011 Oct 21;76(20):8151-8. doi: 10.1021/jo200288t. Epub 2011 Sep 20.

PMID:
21793547
23.

Methyl 2-acetamido-2-deoxy-β-D-glucopyranoside dihydrate and methyl 2-formamido-2-deoxy-β-D-glucopyranoside.

Hu X, Zhang W, Oliver AG, Serianni AS.

Acta Crystallogr C. 2011 Apr;67(Pt 4):o146-50. doi: 10.1107/S0108270111009061. Epub 2011 Mar 22.

PMID:
21467623
24.

A thermal hysteresis-producing xylomannan glycolipid antifreeze associated with cold tolerance is found in diverse taxa.

Walters KR Jr, Serianni AS, Voituron Y, Sformo T, Barnes BM, Duman JG.

J Comp Physiol B. 2011 Jul;181(5):631-40. doi: 10.1007/s00360-011-0552-8. Epub 2011 Jan 30.

PMID:
21279720
25.

Co-crystals of 3-deoxy-3-fluoro-α-D-glucopyranose and 3-deoxy-3-fluoro-β-D-glucopyranose.

Zhang W, Oliver AG, Serianni AS.

Acta Crystallogr C. 2010 Nov;66(Pt 11):o557-60. doi: 10.1107/S0108270110040096. Epub 2010 Oct 21.

26.

4-Deoxy-4-fluoro-β-D-glucopyranose.

Zhang W, Oliver AG, Serianni AS.

Acta Crystallogr C. 2010 Oct;66(Pt 10):o496-8. doi: 10.1107/S0108270110034001. Epub 2010 Sep 4.

27.

Carbohydrate - 25th international symposium.

Serianni AS.

IDrugs. 2010 Oct;13(10):686-8.

PMID:
20878587
28.

Methyl beta-D-galactopyranosyl-(1-->4)-beta-D-allopyranoside tetrahydrate.

Zhang W, Oliver AG, Serianni AS.

Acta Crystallogr C. 2010 Sep;66(Pt 9):o484-7. doi: 10.1107/S0108270110029471. Epub 2010 Aug 21.

PMID:
20814113
29.
30.

1-(beta-D-Erythrofuranosyl)adenosine.

Kline PC, Zhao H, Noll BC, Oliver AG, Serianni AS.

Acta Crystallogr C. 2010 Apr;66(Pt 4):o215-8. doi: 10.1107/S0108270110008024. Epub 2010 Mar 19.

PMID:
20354314
31.

Amide cis-trans isomerization in aqueous solutions of methyl N-formyl-D-glucosaminides and methyl N-acetyl-D-glucosaminides: chemical equilibria and exchange kinetics.

Hu X, Zhang W, Carmichael I, Serianni AS.

J Am Chem Soc. 2010 Apr 7;132(13):4641-52. doi: 10.1021/ja9086787.

PMID:
20225805
32.

Methyl 4-O-beta-D-galactopyranosyl alpha-D-mannopyranoside methanol 0.375-solvate.

Hu X, Pan Q, Noll BC, Oliver AG, Serianni AS.

Acta Crystallogr C. 2010 Feb;66(Pt 2):o67-70. doi: 10.1107/S0108270109055012. Epub 2010 Jan 15.

PMID:
20124684
33.

Methyl beta-allolactoside [methyl beta-D-galactopyranosyl-(1-->6)-beta-D-glucopyranoside] monohydrate.

Klepach TE, Reed M, Noll BC, Oliver AG, Serianni AS.

Acta Crystallogr C. 2009 Dec;65(Pt 12):o601-6. doi: 10.1107/S0108270109042310. Epub 2009 Nov 7.

PMID:
19966440
34.

A nonprotein thermal hysteresis-producing xylomannan antifreeze in the freeze-tolerant Alaskan beetle Upis ceramboides.

Walters KR Jr, Serianni AS, Sformo T, Barnes BM, Duman JG.

Proc Natl Acad Sci U S A. 2009 Dec 1;106(48):20210-5. doi: 10.1073/pnas.0909872106. Epub 2009 Nov 23.

35.

An NMR investigation of putative interresidue H-bonding in methyl alpha-cellobioside in solution.

Zhang W, Zhao H, Carmichael I, Serianni AS.

Carbohydr Res. 2009 Aug 17;344(12):1582-7. doi: 10.1016/j.carres.2009.06.007. Epub 2009 Jun 7.

PMID:
19632671
36.

Cryoprotectant biosynthesis and the selective accumulation of threitol in the freeze-tolerant Alaskan beetle, Upis ceramboides.

Walters KR Jr, Pan Q, Serianni AS, Duman JG.

J Biol Chem. 2009 Jun 19;284(25):16822-31. doi: 10.1074/jbc.M109.013870. Epub 2009 Apr 29.

37.

13C-labeled N-acetyl-neuraminic acid in aqueous solution: detection and quantification of acyclic keto, keto hydrate, and enol forms by 13C NMR spectroscopy.

Klepach T, Carmichael I, Serianni AS.

J Am Chem Soc. 2008 Sep 10;130(36):11892-900. doi: 10.1021/ja077565g. Epub 2008 Aug 19.

PMID:
18710238
38.

(13)C-(1)H and (13)C-(13)C NMR J-couplings in (13)C-labeled N-acetyl-neuraminic acid: correlations with molecular structure.

Klepach T, Zhang W, Carmichael I, Serianni AS.

J Org Chem. 2008 Jun 20;73(12):4376-87. doi: 10.1021/jo702204x. Epub 2008 May 20.

PMID:
18489160
39.

Oligosaccharide trans-glycoside 3JCOCC Karplus curves are not equivalent: effect of internal electronegative substituents.

Zhao H, Carmichael I, Serianni AS.

J Org Chem. 2008 Apr 18;73(8):3255-7. doi: 10.1021/jo702288h. Epub 2008 Mar 20.

PMID:
18351773
40.

Conformational analysis of beta-glycosidic linkages in 13C-labeled glucobiosides using inter-residue scalar coupling constants.

Olsson U, Serianni AS, Stenutz R.

J Phys Chem B. 2008 Apr 10;112(14):4447-53. doi: 10.1021/jp710977k. Epub 2008 Mar 18.

PMID:
18345660
41.

Pyridoxamine protects proteins from functional damage by 3-deoxyglucosone: mechanism of action of pyridoxamine.

Chetyrkin SV, Zhang W, Hudson BG, Serianni AS, Voziyan PA.

Biochemistry. 2008 Jan 22;47(3):997-1006. Epub 2007 Dec 28.

PMID:
18161948
42.

3-Deoxy-beta-D-ribo-hexopyranose (3-deoxy-beta-D-glucopyranose).

Zhang W, Noll BC, Serianni AS.

Acta Crystallogr C. 2007 Oct;63(Pt 10):o578-81. Epub 2007 Sep 1.

PMID:
17917226
43.

13C-13C NMR spin-spin coupling constants in saccharides: structural correlations involving all carbons in aldohexopyranosyl rings.

Bose-Basu B, Klepach T, Bondo G, Bondo PB, Zhang W, Carmichael I, Serianni AS.

J Org Chem. 2007 Sep 28;72(20):7511-22. Epub 2007 Sep 7.

PMID:
17824645
44.

A disaccharide rearrangement catalyzed by molybdate anion in aqueous solution.

Wu Q, Pan Q, Zhao S, Imker H, Serianni AS.

J Org Chem. 2007 Apr 13;72(8):3081-4. Epub 2007 Mar 20.

PMID:
17371071
45.

DFT and NMR studies of 2JCOH, 3JHCOH, and 3JCCOH spin-couplings in saccharides: C-O torsional bias and H-bonding in aqueous solution.

Zhao H, Pan Q, Zhang W, Carmichael I, Serianni AS.

J Org Chem. 2007 Sep 14;72(19):7071-82. Epub 2007 Feb 23.

PMID:
17316047
46.

1-(beta-D-Erythrofuranosyl)cytidine (beta-erythrocytidine).

Kline PC, Noll BC, Zhao H, Serianni AS.

Acta Crystallogr C. 2007 Feb;63(Pt 2):o137-40. Epub 2007 Jan 23. No abstract available.

PMID:
17284809
47.

1JCH correlates with alcohol hydrogen bond strength.

Maiti NC, Zhu Y, Carmichael I, Serianni AS, Anderson VE.

J Org Chem. 2006 Mar 31;71(7):2878-80.

PMID:
16555846
48.

Methyl 4-O-beta-L-galactopyranosyl-beta-D-glucopyranoside (methyl beta-L-lactoside).

Pan Q, Noll BC, Serianni AS.

Acta Crystallogr C. 2006 Feb;62(Pt 2):o82-5. Epub 2006 Jan 21.

PMID:
16456293
49.

[13C,15N]2-Acetamido-2-deoxy-D-aldohexoses and their methyl glycosides: synthesis and NMR investigations of J-couplings involving 1H, 13C, and 15N.

Zhu Y, Pan Q, Thibaudeau C, Zhao S, Carmichael I, Serianni AS.

J Org Chem. 2006 Jan 20;71(2):466-79.

PMID:
16408953
50.

Comparative overwintering physiology of Alaska and Indiana populations of the beetle Cucujus clavipes (Fabricius): roles of antifreeze proteins, polyols, dehydration and diapause.

Bennett VA, Sformo T, Walters K, Tøien Ø, Jeannet K, Hochstrasser R, Pan Q, Serianni AS, Barnes BM, Duman JG.

J Exp Biol. 2005 Dec;208(Pt 23):4467-77.

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