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Items: 1 to 50 of 105

1.

Compromise in uncertainty estimation by modelling and validation approaches for an HPLC-UV method for measurement of biochemical indicators of vitamins A and E.

Djellouli O, Rozet E, Dahmani B, Hubert P.

Analyst. 2018 Mar 12;143(6):1492-1501. doi: 10.1039/c7an01804e.

PMID:
29488516
2.

Fingerprinting and validation of a LC-DAD method for the analysis of biflavanones in Garcinia kola-based antimalarial improved traditional medicines.

Tshibangu PT, Kapepula PM, Kapinga MJK, Lupona HK, Ngombe NK, Kalenda DT, Jansen O, Wauters JN, Tits M, Angenot L, Rozet E, Hubert P, Marini RD, Frédérich M.

J Pharm Biomed Anal. 2016 Sep 5;128:382-390. doi: 10.1016/j.jpba.2016.04.042. Epub 2016 Jun 9.

PMID:
27343901
3.

Understanding the impact of microcrystalline cellulose physicochemical properties on tabletability.

Thoorens G, Krier F, Rozet E, Carlin B, Evrard B.

Int J Pharm. 2015 Jul 25;490(1-2):47-54. doi: 10.1016/j.ijpharm.2015.05.026. Epub 2015 May 14.

PMID:
25981619
4.

Towards a full integration of optimization and validation phases: An analytical-quality-by-design approach.

Hubert C, Houari S, Rozet E, Lebrun P, Hubert P.

J Chromatogr A. 2015 May 22;1395:88-98. doi: 10.1016/j.chroma.2015.03.059. Epub 2015 Mar 30.

5.

Estimation of the Time Interval between the Administration of Heroin and the Sampling of Blood in Chronic Inhalers.

Dubois N, Hallet C, Seidel L, Demaret I, Luppens D, Ansseau M, Rozet E, Albert A, Hubert P, Charlier C.

J Anal Toxicol. 2015 May;39(4):300-5. doi: 10.1093/jat/bkv001. Epub 2015 Feb 3.

PMID:
25648554
6.

A quality by design approach for longitudinal quality attributes.

Lebrun P, Giacoletti K, Scherder T, Rozet E, Boulanger B.

J Biopharm Stat. 2015;25(2):247-59. doi: 10.1080/10543406.2014.979197.

7.

Analytical procedure validation and the quality by design paradigm.

Rozet E, Lebrun P, Michiels JF, Sondag P, Scherder T, Boulanger B.

J Biopharm Stat. 2015;25(2):260-8. doi: 10.1080/10543406.2014.971176.

8.

A new criterion to assess distributional homogeneity in hyperspectral images of solid pharmaceutical dosage forms.

Sacré PY, Lebrun P, Chavez PF, De Bleye C, Netchacovitch L, Rozet E, Klinkenberg R, Streel B, Hubert P, Ziemons E.

Anal Chim Acta. 2014 Mar 25;818:7-14. doi: 10.1016/j.aca.2014.02.014. Epub 2014 Feb 12.

9.

Strategies for using the sheep ovarian cortex as a model in reproductive medicine.

Fransolet M, Labied S, Henry L, Masereel MC, Rozet E, Kirschvink N, Nisolle M, Munaut C.

PLoS One. 2014 Mar 10;9(3):e91073. doi: 10.1371/journal.pone.0091073. eCollection 2014.

10.

Plasma level monitoring of the major metabolites of diacetylmorphine (heroin) by the "chasing the dragon" route in severe heroin addicts.

Dubois N, Demaret I, Ansseau M, Rozet E, Hubert P, Charlier C.

Acta Clin Belg. 2013 Sep-Oct;68(5):359-67.

PMID:
24579243
11.

Evaluation of the quantitative performances of supercritical fluid chromatography: from method development to validation.

Dispas A, Lebrun P, Ziemons E, Marini R, Rozet E, Hubert P.

J Chromatogr A. 2014 Aug 1;1353:78-88. doi: 10.1016/j.chroma.2014.01.046. Epub 2014 Jan 24.

PMID:
24513349
12.

An easy, convenient cell and tissue extraction protocol for nuclear magnetic resonance metabolomics.

Matheus N, Hansen S, Rozet E, Peixoto P, Maquoi E, Lambert V, Noël A, Frédérich M, Mottet D, de Tullio P.

Phytochem Anal. 2014 Jul-Aug;25(4):342-9. doi: 10.1002/pca.2498. Epub 2014 Jan 23.

PMID:
24453161
13.

Fast method for the simultaneous quantification of toxic polyphenols applied to the selection of genotypes of yam bean (Pachyrhizus sp.) seeds.

Lautié E, Rozet E, Hubert P, Vandelaer N, Billard F, Felde TZ, Grüneberg WJ, Quetin-Leclercq J.

Talanta. 2013 Dec 15;117:94-101. doi: 10.1016/j.talanta.2013.08.038. Epub 2013 Sep 3.

PMID:
24209316
14.

Robust method optimization strategy-a useful tool for method transfer: the case of SFC.

Dispas A, Lebrun P, Andri B, Rozet E, Hubert P.

J Pharm Biomed Anal. 2014 Jan;88:519-24. doi: 10.1016/j.jpba.2013.09.030. Epub 2013 Oct 12.

PMID:
24184381
15.

Development of a liquid chromatographic method for the simultaneous quantification of curcumin, β-arteether, tetrahydrocurcumin and dihydroartemisinin. Application to lipid-based formulations.

Memvanga PB, Mbinze JK, Rozet E, Hubert P, Préat V, Marini RD.

J Pharm Biomed Anal. 2014 Jan;88:447-56. doi: 10.1016/j.jpba.2013.09.009. Epub 2013 Oct 5.

PMID:
24184380
16.

Improvement of a stability-indicating method by Quality-by-Design versus Quality-by-Testing: a case of a learning process.

Hubert C, Lebrun P, Houari S, Ziemons E, Rozet E, Hubert P.

J Pharm Biomed Anal. 2014 Jan;88:401-9. doi: 10.1016/j.jpba.2013.09.026. Epub 2013 Oct 5.

PMID:
24176744
17.

PAT tools for the control of co-extrusion implants manufacturing process.

Krier F, Mantanus J, Sacré PY, Chavez PF, Thiry J, Pestieau A, Rozet E, Ziemons E, Hubert P, Evrard B.

Int J Pharm. 2013 Dec 15;458(1):15-24. doi: 10.1016/j.ijpharm.2013.09.040. Epub 2013 Oct 19.

PMID:
24148661
18.

Determination of 4-aminophenol in a pharmaceutical formulation using surface enhanced Raman scattering: from development to method validation.

De Bleye C, Dumont E, Rozet E, Sacré PY, Chavez PF, Netchacovitch L, Piel G, Hubert P, Ziemons E.

Talanta. 2013 Nov 15;116:899-905. doi: 10.1016/j.talanta.2013.07.084. Epub 2013 Aug 12.

PMID:
24148492
19.

Laser-induced choroidal neovascularization model to study age-related macular degeneration in mice.

Lambert V, Lecomte J, Hansen S, Blacher S, Gonzalez ML, Struman I, Sounni NE, Rozet E, de Tullio P, Foidart JM, Rakic JM, Noel A.

Nat Protoc. 2013 Nov;8(11):2197-211. doi: 10.1038/nprot.2013.135. Epub 2013 Oct 17.

20.

Development and validation of an UHPLC-LTQ-Orbitrap MS method for non-anthocyanin flavonoids quantification in Euterpe oleracea juice.

Dias AL, Rozet E, Larondelle Y, Hubert P, Rogez H, Quetin-Leclercq J.

Anal Bioanal Chem. 2013 Nov;405(28):9235-49. doi: 10.1007/s00216-013-7325-z. Epub 2013 Oct 18.

PMID:
24136248
21.

Influence of sample and mobile phase composition on peptide retention behaviour and sensitivity in reversed-phase liquid chromatography/mass spectrometry.

Houbart V, Rozet E, Matagne A, Crommen J, Servais AC, Fillet M.

J Chromatogr A. 2013 Nov 1;1314:199-207. doi: 10.1016/j.chroma.2013.09.036. Epub 2013 Sep 13.

PMID:
24070623
22.

Application of an innovative design space optimization strategy to the development of LC methods for the simultaneous screening of antibiotics to combat poor quality medicines.

Mbinze JK, Dispas A, Lebrun P, Mavar Tayey Mbay J, Habyalimana V, Kalenda N, Rozet E, Hubert P, Marini RD.

J Pharm Biomed Anal. 2013 Nov;85:83-92. doi: 10.1016/j.jpba.2013.06.036. Epub 2013 Jul 12.

PMID:
23912056
23.

Experimental in situ exposure of the seagrass Posidonia oceanica (L.) Delile to 15 trace elements.

Richir J, Luy N, Lepoint G, Rozet E, Alvera Azcarate A, Gobert S.

Aquat Toxicol. 2013 Sep 15;140-141:157-73. doi: 10.1016/j.aquatox.2013.05.018. Epub 2013 Jun 3.

24.

Usefulness of information criteria for the selection of calibration curves.

Rozet E, Ziemons E, Marini RD, Hubert P.

Anal Chem. 2013 Jul 2;85(13):6327-35. doi: 10.1021/ac400630k. Epub 2013 Jun 18.

PMID:
23777474
25.

Enzymatic but not compensated Jaffe methods reach the desirable specifications of NKDEP at normal levels of creatinine. Results of the French multicentric evaluation.

Boutten A, Bargnoux AS, Carlier MC, Delanaye P, Rozet E, Delatour V, Cavalier E, Hanser AM, Froissart M, Cristol JP, Piéroni L; Société Française de Biologie Clinique.

Clin Chim Acta. 2013 Apr 18;419:132-5. doi: 10.1016/j.cca.2013.01.021. Epub 2013 Feb 13.

PMID:
23415696
26.

Fast microwave-assisted extraction of rotenone for its quantification in seeds of yam bean (Pachyrhizus sp.).

Lautié E, Rasse C, Rozet E, Mourgues C, Vanhelleputte JP, Quetin-Leclercq J.

J Sep Sci. 2013 Feb;36(4):758-63. doi: 10.1002/jssc.201200347. Epub 2013 Jan 22.

PMID:
23341347
27.

Methodology for the validation of analytical methods involved in uniformity of dosage units tests.

Rozet E, Ziemons E, Marini RD, Boulanger B, Hubert P.

Anal Chim Acta. 2013 Jan 14;760:46-52. doi: 10.1016/j.aca.2012.11.013. Epub 2012 Nov 16.

PMID:
23265732
28.

Implementation of a design space approach for enantiomeric separations in polar organic solvent chromatography.

Nistor I, Lebrun P, Ceccato A, Lecomte F, Slama I, Oprean R, Badarau E, Dufour F, Dossou KS, Fillet M, Liégeois JF, Hubert P, Rozet E.

J Pharm Biomed Anal. 2013 Feb 23;74:273-83. doi: 10.1016/j.jpba.2012.10.015. Epub 2012 Nov 2.

PMID:
23245261
29.

Reply to the responses on the comments on "Uncertainty profiles for the validation of analytical methods" by Saffaj and Ihssane.

Rozet E, Ziemons E, Marini RD, Boulanger B, Hubert P, Boulanger B.

Talanta. 2012 Oct 15;100:290-2. doi: 10.1016/j.talanta.2012.07.047. Epub 2012 Aug 2.

PMID:
23141339
30.

Validation of analytical methods involved in dissolution assays: acceptance limits and decision methodologies.

Rozet E, Ziemons E, Marini RD, Boulanger B, Hubert P.

Anal Chim Acta. 2012 Nov 2;751:44-51. doi: 10.1016/j.aca.2012.09.017. Epub 2012 Sep 20.

PMID:
23084050
31.

Application of an innovative design space optimization strategy to the development of liquid chromatographic methods to combat potentially counterfeit nonsteroidal anti-inflammatory drugs.

Mbinze JK, Lebrun P, Debrus B, Dispas A, Kalenda N, Mavar Tayey Mbay J, Schofield T, Boulanger B, Rozet E, Hubert P, Marini RD.

J Chromatogr A. 2012 Nov 9;1263:113-24. doi: 10.1016/j.chroma.2012.09.038. Epub 2012 Sep 20.

PMID:
23046622
32.

A rapid validated UHPLC-PDA method for anthocyanins quantification from Euterpe oleracea fruits.

Dias AL, Rozet E, Chataigné G, Oliveira AC, Rabelo CA, Hubert P, Rogez H, Quetin-Leclercq J.

J Chromatogr B Analyt Technol Biomed Life Sci. 2012 Oct 15;907:108-16. doi: 10.1016/j.jchromb.2012.09.015. Epub 2012 Sep 16.

PMID:
23026226
33.

Flexibility and applicability of β-expectation tolerance interval approach to assess the fitness of purpose of pharmaceutical analytical methods.

Bouabidi A, Talbi M, Bourichi H, Bouklouze A, El Karbane M, Boulanger B, Brik Y, Hubert P, Rozet E.

Drug Test Anal. 2012 Dec;4(12):1014-27. doi: 10.1002/dta.1345. Epub 2012 May 21.

PMID:
22615163
34.

New methodology for the development of chromatographic methods with bioanalytical application.

Rozet E, Lebrun P, Debrus B, Hubert P.

Bioanalysis. 2012 Apr;4(7):755-8. doi: 10.4155/bio.12.47. No abstract available.

35.

Critical review of near-infrared spectroscopic methods validations in pharmaceutical applications.

De Bleye C, Chavez PF, Mantanus J, Marini R, Hubert P, Rozet E, Ziemons E.

J Pharm Biomed Anal. 2012 Oct;69:125-32. doi: 10.1016/j.jpba.2012.02.003. Epub 2012 Mar 7. Review.

PMID:
22464561
36.

Application of design of experiments and design space methodology for the HPLC-UV separation optimization of aporphine alkaloids from leaves of Spirospermum penduliflorum Thouars.

Rafamantanana MH, Debrus B, Raoelison GE, Rozet E, Lebrun P, Uverg-Ratsimamanga S, Hubert P, Quetin-Leclercq J.

J Pharm Biomed Anal. 2012 Mar 25;62:23-32. doi: 10.1016/j.jpba.2011.12.028. Epub 2012 Jan 25.

PMID:
22310553
37.

Comments on "uncertainty profiles for the validation of analytical methods" by Saffaj and Ihssane.

Rozet E, Ziemons E, Marini RD, Boulanger B, Hubert P.

Talanta. 2012 Jan 15;88:769-71. doi: 10.1016/j.talanta.2011.11.011. Epub 2011 Nov 6. No abstract available.

PMID:
22265573
38.

Usefulness of capability indices in the framework of analytical methods validation.

Bouabidi A, Ziemons E, Marini R, Hubert C, Talbi M, Bouklouze A, Bourichi H, El Karbane M, Boulanger B, Hubert P, Rozet E.

Anal Chim Acta. 2012 Feb 10;714:47-56. doi: 10.1016/j.aca.2011.11.019. Epub 2011 Dec 6.

PMID:
22244136
39.

Comparison of acid and enzymatic methods for inulin dosage: analytical performances and impact on glomerular filtration rate evaluation.

Delanaye P, Thibaudin L, Souvignet M, Maillard N, Alamartine E, Rozet E, Cavalier E, Mariat C.

Clin Chim Acta. 2012 Mar 22;413(5-6):556-60. doi: 10.1016/j.cca.2011.11.024. Epub 2011 Dec 1.

PMID:
22155341
40.

Quality by design compliant analytical method validation.

Rozet E, Ziemons E, Marini RD, Boulanger B, Hubert P.

Anal Chem. 2012 Jan 3;84(1):106-12. doi: 10.1021/ac202664s. Epub 2011 Dec 8.

PMID:
22107128
41.

Design space approach in the optimization of the spray-drying process.

Lebrun P, Krier F, Mantanus J, Grohganz H, Yang M, Rozet E, Boulanger B, Evrard B, Rantanen J, Hubert P.

Eur J Pharm Biopharm. 2012 Jan;80(1):226-34. doi: 10.1016/j.ejpb.2011.09.014. Epub 2011 Sep 29.

PMID:
21983606
42.

Evaluating the reliability of analytical results using a probability criterion: a Bayesian perspective.

Rozet E, Govaerts B, Lebrun P, Michail K, Ziemons E, Wintersteiger R, Rudaz S, Boulanger B, Hubert P.

Anal Chim Acta. 2011 Oct 31;705(1-2):193-206. doi: 10.1016/j.aca.2011.05.028. Epub 2011 May 23.

PMID:
21962362
43.

Comparison of the quantitative performances and measurement uncertainty estimates obtained during method validation versus routine applications of a novel hydrophilic interaction chromatography method for the determination of cidofovir in human plasma.

Lecomte F, Hubert C, Demarche S, De Bleye C, Dispas A, Jost M, Frankenne F, Ceccato A, Rozet E, Hubert P.

J Pharm Biomed Anal. 2012 Jan 5;57:153-65. doi: 10.1016/j.jpba.2011.08.040. Epub 2011 Sep 10.

PMID:
21959349
44.

Models to estimate overall analytical measurements uncertainty: assumptions, comparisons and applications.

Rozet E, Rudaz S, Marini RD, Ziémons E, Boulanger B, Hubert P.

Anal Chim Acta. 2011 Sep 30;702(2):160-71. doi: 10.1016/j.aca.2011.06.055. Epub 2011 Jul 5. Review.

PMID:
21839193
45.

Development and validation of a ultra-high-performance liquid chromatography-UV method for the detection and quantification of erectile dysfunction drugs and some of their analogues found in counterfeit medicines.

Sacré PY, Deconinck E, Chiap P, Crommen J, Mansion F, Rozet E, Courselle P, De Beer JO.

J Chromatogr A. 2011 Sep 16;1218(37):6439-47. doi: 10.1016/j.chroma.2011.07.029. Epub 2011 Jul 20.

46.

A multicentric evaluation of IDMS-traceable creatinine enzymatic assays.

Piéroni L, Delanaye P, Boutten A, Bargnoux AS, Rozet E, Delatour V, Carlier MC, Hanser AM, Cavalier E, Froissart M, Cristol JP; Société Française de Biologie Clinique.

Clin Chim Acta. 2011 Nov 20;412(23-24):2070-5. doi: 10.1016/j.cca.2011.07.012. Epub 2011 Jul 22.

47.

Innovative high-performance liquid chromatography method development for the screening of 19 antimalarial drugs based on a generic approach, using design of experiments, independent component analysis and design space.

Debrus B, Lebrun P, Kindenge JM, Lecomte F, Ceccato A, Caliaro G, Mbay JM, Boulanger B, Marini RD, Rozet E, Hubert P.

J Chromatogr A. 2011 Aug 5;1218(31):5205-15. doi: 10.1016/j.chroma.2011.05.102. Epub 2011 Jun 12.

PMID:
21705006
48.

Near infrared and Raman spectroscopy as Process Analytical Technology tools for the manufacturing of silicone-based drug reservoirs.

Mantanus J, Rozet E, Van Butsele K, De Bleye C, Ceccato A, Evrard B, Hubert P, Ziémons E.

Anal Chim Acta. 2011 Aug 5;699(1):96-106. doi: 10.1016/j.aca.2011.05.006. Epub 2011 May 11.

PMID:
21704763
49.

Application of a new optimization strategy for the separation of tertiary alkaloids extracted from Strychnos usambarensis leaves.

Nistor I, Cao M, Debrus B, Lebrun P, Lecomte F, Rozet E, Angenot L, Frederich M, Oprean R, Hubert P.

J Pharm Biomed Anal. 2011 Aug 25;56(1):30-7. doi: 10.1016/j.jpba.2011.04.027. Epub 2011 May 7.

PMID:
21628087
50.

Validation, transfer and measurement uncertainty estimation of an HPLC-UV method for the quantification of artemisinin in hydro alcoholic extracts of Artemisia annua L.

Diawara HZ, Gbaguidi F, Evrard B, Leclercq JQ, Moudachirou M, Debrus B, Hubert P, Rozet E.

J Pharm Biomed Anal. 2011 Aug 25;56(1):7-15. doi: 10.1016/j.jpba.2011.04.012. Epub 2011 Apr 21.

PMID:
21570794

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