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Items: 36

1.

Protein resonance assignment by BSH-CP-based 3D solid-state NMR experiments: A practical guide.

Hoffmann J, Ruta J, Shi C, Hendriks K, Chevelkov V, Franks WT, Oschkinat H, Giller K, Becker S, Lange A.

Magn Reson Chem. 2019 Nov 5. doi: 10.1002/mrc.4945. [Epub ahead of print]

PMID:
31691361
2.

Structure and Dynamics of the Rhomboid Protease GlpG in Liposomes Studied by Solid-State NMR.

Shi C, Öster C, Bohg C, Li L, Lange S, Chevelkov V, Lange A.

J Am Chem Soc. 2019 Oct 30;141(43):17314-17321. doi: 10.1021/jacs.9b08952. Epub 2019 Oct 16.

PMID:
31603315
3.

The conduction pathway of potassium channels is water free under physiological conditions.

Öster C, Hendriks K, Kopec W, Chevelkov V, Shi C, Michl D, Lange S, Sun H, de Groot BL, Lange A.

Sci Adv. 2019 Jul 31;5(7):eaaw6756. doi: 10.1126/sciadv.aaw6756. eCollection 2019 Jul.

4.

Characterization of H/D exchange in type 1 pili by proton-detected solid-state NMR and molecular dynamics simulations.

Hwang S, Öster C, Chevelkov V, Giller K, Lange S, Becker S, Lange A.

J Biomol NMR. 2019 Jul;73(6-7):281-291. doi: 10.1007/s10858-019-00247-3. Epub 2019 Apr 26.

5.

Structure determination of supra-molecular assemblies by solid-state NMR: Practical considerations.

Demers JP, Fricke P, Shi C, Chevelkov V, Lange A.

Prog Nucl Magn Reson Spectrosc. 2018 Dec;109:51-78. doi: 10.1016/j.pnmrs.2018.06.002. Epub 2018 Jun 18. Review.

PMID:
30527136
6.

Measurement of backbone hydrogen-deuterium exchange in the type III secretion system needle protein PrgI by solid-state NMR.

Chevelkov V, Giller K, Becker S, Lange A.

J Magn Reson. 2017 Oct;283:110-116. doi: 10.1016/j.jmr.2017.08.012. Epub 2017 Sep 1.

7.

Backbone assignment of perdeuterated proteins by solid-state NMR using proton detection and ultrafast magic-angle spinning.

Fricke P, Chevelkov V, Zinke M, Giller K, Becker S, Lange A.

Nat Protoc. 2017 Apr;12(4):764-782. doi: 10.1038/nprot.2016.190. Epub 2017 Mar 9.

PMID:
28277547
8.

High resolution observed in 800 MHz DNP spectra of extremely rigid type III secretion needles.

Fricke P, Mance D, Chevelkov V, Giller K, Becker S, Baldus M, Lange A.

J Biomol NMR. 2016 Aug;65(3-4):121-126. doi: 10.1007/s10858-016-0044-y. Epub 2016 Jun 28.

PMID:
27351550
9.

Atomic-resolution structure of cytoskeletal bactofilin by solid-state NMR.

Shi C, Fricke P, Lin L, Chevelkov V, Wegstroth M, Giller K, Becker S, Thanbichler M, Lange A.

Sci Adv. 2015 Dec 4;1(11):e1501087. doi: 10.1126/sciadv.1501087. eCollection 2015 Dec.

10.

Perspectives for sensitivity enhancement in proton-detected solid-state NMR of highly deuterated proteins by preserving water magnetization.

Chevelkov V, Xiang S, Giller K, Becker S, Lange A, Reif B.

J Biomol NMR. 2015 Feb;61(2):151-60. doi: 10.1007/s10858-015-9902-2. Epub 2015 Jan 30.

PMID:
25634300
11.

Specific 13C labeling of leucine, valine and isoleucine methyl groups for unambiguous detection of long-range restraints in protein solid-state NMR studies.

Fasshuber HK, Demers JP, Chevelkov V, Giller K, Becker S, Lange A.

J Magn Reson. 2015 Mar;252:10-9. doi: 10.1016/j.jmr.2014.12.013. Epub 2015 Jan 6.

PMID:
25625825
12.

Strategies for solid-state NMR investigations of supramolecular assemblies with large subunit sizes.

Fricke P, Chevelkov V, Shi C, Lange A.

J Magn Reson. 2015 Apr;253:2-9. doi: 10.1016/j.jmr.2014.10.018. Epub 2014 Nov 15.

PMID:
25487122
13.

Towards automatic protein backbone assignment using proton-detected 4D solid-state NMR data.

Xiang S, Chevelkov V, Becker S, Lange A.

J Biomol NMR. 2014 Nov;60(2-3):85-90. doi: 10.1007/s10858-014-9859-6. Epub 2014 Sep 6.

PMID:
25193427
14.

Proton-detected MAS NMR experiments based on dipolar transfers for backbone assignment of highly deuterated proteins.

Chevelkov V, Habenstein B, Loquet A, Giller K, Becker S, Lange A.

J Magn Reson. 2014 May;242:180-8. doi: 10.1016/j.jmr.2014.02.020. Epub 2014 Mar 4.

PMID:
24667274
15.

BSH-CP based 3D solid-state NMR experiments for protein resonance assignment.

Shi C, Fasshuber HK, Chevelkov V, Xiang S, Habenstein B, Vasa SK, Becker S, Lange A.

J Biomol NMR. 2014 May;59(1):15-22. doi: 10.1007/s10858-014-9820-8. Epub 2014 Mar 1.

PMID:
24584701
16.

Synthetic access to a hydrocarbon-soluble trifluorinated Ge(II) compound and its Sn(II) congener.

Samuel PP, Li Y, Roesky HW, Chevelkov V, Lange A, Burkhardt A, Dittrich B.

J Am Chem Soc. 2014 Jan 29;136(4):1292-5. doi: 10.1021/ja412151e. Epub 2014 Jan 16.

PMID:
24433048
17.

Atomic structure and handedness of the building block of a biological assembly.

Loquet A, Habenstein B, Chevelkov V, Vasa SK, Giller K, Becker S, Lange A.

J Am Chem Soc. 2013 Dec 26;135(51):19135-8. doi: 10.1021/ja411362q. Epub 2013 Dec 17.

PMID:
24328247
18.

Internal protein dynamics on ps to μs timescales as studied by multi-frequency (15)N solid-state NMR relaxation.

Zinkevich T, Chevelkov V, Reif B, Saalwächter K, Krushelnitsky A.

J Biomol NMR. 2013 Nov;57(3):219-35. doi: 10.1007/s10858-013-9782-2. Epub 2013 Sep 19.

PMID:
24048638
19.

Efficient band-selective homonuclear CO-CA cross-polarization in protonated proteins.

Chevelkov V, Shi C, Fasshuber HK, Becker S, Lange A.

J Biomol NMR. 2013 Aug;56(4):303-11. doi: 10.1007/s10858-013-9767-1. Epub 2013 Aug 8.

PMID:
23925478
20.

Efficient CO-CA transfer in highly deuterated proteins by band-selective homonuclear cross-polarization.

Chevelkov V, Giller K, Becker S, Lange A.

J Magn Reson. 2013 May;230:205-11. doi: 10.1016/j.jmr.2013.02.021. Epub 2013 Mar 15.

PMID:
23558259
21.

Lewis base mediated dismutation of trichlorosilane.

Singh AP, Ghadwal RS, Roesky HW, Holstein JJ, Dittrich B, Demers JP, Chevelkov V, Lange A.

Chem Commun (Camb). 2012 Aug 7;48(61):7574-6. doi: 10.1039/c2cc33835a. Epub 2012 Jun 26.

PMID:
22735667
22.

Progress in correlation spectroscopy at ultra-fast magic-angle spinning: basic building blocks and complex experiments for the study of protein structure and dynamics.

Demers JP, Chevelkov V, Lange A.

Solid State Nucl Magn Reson. 2011 Oct;40(3):101-13. doi: 10.1016/j.ssnmr.2011.07.002. Epub 2011 Aug 3. Review.

PMID:
21880471
23.

Microsecond time scale mobility in a solid protein as studied by the 15N R(1rho) site-specific NMR relaxation rates.

Krushelnitsky A, Zinkevich T, Reichert D, Chevelkov V, Reif B.

J Am Chem Soc. 2010 Sep 1;132(34):11850-3. doi: 10.1021/ja103582n.

PMID:
20690699
24.

Comparison of solid-state dipolar couplings and solution relaxation data provides insight into protein backbone dynamics.

Chevelkov V, Xue Y, Linser R, Skrynnikov NR, Reif B.

J Am Chem Soc. 2010 Apr 14;132(14):5015-7. doi: 10.1021/ja100645k.

PMID:
20297847
25.

15N H/D-SOLEXSY experiment for accurate measurement of amide solvent exchange rates: application to denatured drkN SH3.

Chevelkov V, Xue Y, Rao DK, Forman-Kay JD, Skrynnikov NR.

J Biomol NMR. 2010 Mar;46(3):227-44. doi: 10.1007/s10858-010-9398-8. Epub 2010 Feb 27.

PMID:
20195703
26.

Accurate determination of order parameters from 1H,15N dipolar couplings in MAS solid-state NMR experiments.

Chevelkov V, Fink U, Reif B.

J Am Chem Soc. 2009 Oct 7;131(39):14018-22. doi: 10.1021/ja902649u.

PMID:
19743845
27.

Quantitative analysis of backbone motion in proteins using MAS solid-state NMR spectroscopy.

Chevelkov V, Fink U, Reif B.

J Biomol NMR. 2009 Sep;45(1-2):197-206. doi: 10.1007/s10858-009-9348-5. Epub 2009 Jul 24.

PMID:
19629713
28.

Measurement of 15N-T1 relaxation rates in a perdeuterated protein by magic angle spinning solid-state nuclear magnetic resonance spectroscopy.

Chevelkov V, Diehl A, Reif B.

J Chem Phys. 2008 Feb 7;128(5):052316. doi: 10.1063/1.2819311.

PMID:
18266433
29.
30.

Sensitivity enhancement using paramagnetic relaxation in MAS solid-state NMR of perdeuterated proteins.

Linser R, Chevelkov V, Diehl A, Reif B.

J Magn Reson. 2007 Dec;189(2):209-16. Epub 2007 Sep 18.

PMID:
17923428
31.

Combined analysis of (15)N relaxation data from solid- and solution-state NMR spectroscopy.

Chevelkov V, Zhuravleva AV, Xue Y, Reif B, Skrynnikov NR.

J Am Chem Soc. 2007 Oct 24;129(42):12594-5. Epub 2007 Sep 29. No abstract available.

PMID:
17902660
32.

Differential line broadening in MAS solid-state NMR due to dynamic interference.

Chevelkov V, Faelber K, Schrey A, Rehbein K, Diehl A, Reif B.

J Am Chem Soc. 2007 Aug 22;129(33):10195-200. Epub 2007 Jul 31.

PMID:
17663552
33.

Ultrahigh resolution in proton solid-state NMR spectroscopy at high levels of deuteration.

Chevelkov V, Rehbein K, Diehl A, Reif B.

Angew Chem Int Ed Engl. 2006 Jun 2;45(23):3878-81. No abstract available.

PMID:
16646097
34.

Detection of dynamic water molecules in a microcrystalline sample of the SH3 domain of alpha-spectrin by MAS solid-state NMR.

Chevelkov V, Faelber K, Diehl A, Heinemann U, Oschkinat H, Reif B.

J Biomol NMR. 2005 Apr;31(4):295-310.

PMID:
15928996
35.

Resolution enhancement in MAS solid-state NMR by application of 13C homonuclear scalar decoupling during acquisition.

Chevelkov V, Chen Z, Bermel W, Reif B.

J Magn Reson. 2005 Jan;172(1):56-62.

PMID:
15589408
36.

1H detection in MAS solid-state NMR spectroscopy of biomacromolecules employing pulsed field gradients for residual solvent suppression.

Chevelkov V, van Rossum BJ, Castellani F, Rehbein K, Diehl A, Hohwy M, Steuernagel S, Engelke F, Oschkinat H, Reif B.

J Am Chem Soc. 2003 Jul 2;125(26):7788-9.

PMID:
12822982

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