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Items: 1 to 50 of 107

1.

Ni-catalyzed 1,2-benzylboration of 1,2-disubstituted unactivated alkenes.

Joung S, Bergmann AM, Brown MK.

Chem Sci. 2019 Oct 22;10(47):10944-10947. doi: 10.1039/c9sc04199k. eCollection 2019 Dec 21.

2.

A Workshop Report on the Causes and Consequences of Sleep Health Disparities.

Jackson CL, Walker JR, Brown MK, Das R, Jones NL.

Sleep. 2020 Mar 10. pii: zsaa037. doi: 10.1093/sleep/zsaa037. [Epub ahead of print]

PMID:
32154560
3.

Evolution of a Strategy for the Enantioselective Synthesis of (-)-Cajanusine.

Guo R, Witherspoon BP, Brown MK.

J Am Chem Soc. 2020 Mar 18;142(11):5002-5006. doi: 10.1021/jacs.0c00359. Epub 2020 Mar 9.

PMID:
32149511
4.

NIH Research Conference on Sleep and the Health of Women.

Brown MK, Laposky AD, Buckler AG, Perrotte BM, Parthasarathy S, Twery MJ, Sharkey K.

J Womens Health (Larchmt). 2020 Mar;29(3):427-429. doi: 10.1089/jwh.2020.8341. Epub 2020 Feb 27. No abstract available.

PMID:
32105511
5.

Perfect timing: circadian rhythms, sleep, and immunity - an NIH workshop summary.

Haspel JA, Anafi R, Brown MK, Cermakian N, Depner C, Desplats P, Gelman AE, Haack M, Jelic S, Kim BS, Laposky AD, Lee YC, Mongodin E, Prather AA, Prendergast BJ, Reardon C, Shaw AC, Sengupta S, Szentirmai É, Thakkar M, Walker WE, Solt LA.

JCI Insight. 2020 Jan 16;5(1). pii: 131487. doi: 10.1172/jci.insight.131487. Review.

6.

Lessons in Strain and Stability: Enantioselective Synthesis of (+)-[5]-Ladderanoic Acid.

Hancock EN, Kuker EL, Tantillo DJ, Brown MK.

Angew Chem Int Ed Engl. 2020 Jan 2;59(1):436-441. doi: 10.1002/anie.201910901. Epub 2019 Nov 18.

PMID:
31650679
7.

Nickel-Catalyzed Arylboration of Alkenylarenes: Synthesis of Boron-Substituted Quaternary Carbons and Regiodivergent Reactions.

Chen LA, Lear AR, Gao P, Brown MK.

Angew Chem Int Ed Engl. 2019 Aug 5;58(32):10956-10960. doi: 10.1002/anie.201904861. Epub 2019 Jun 28.

PMID:
31250959
8.

Ni-Catalyzed Arylboration of Unactivated Alkenes: Scope and Mechanistic Studies.

Sardini SR, Lambright AL, Trammel GL, Omer HM, Liu P, Brown MK.

J Am Chem Soc. 2019 Jun 12;141(23):9391-9400. doi: 10.1021/jacs.9b03991. Epub 2019 Jun 4.

PMID:
31184148
9.

(Hetero)arylboration of alkynes: a strategy for the synthesis of α,α-bis(hetero)arylketones.

Huang Y, Bergmann AM, Brown MK.

Org Biomol Chem. 2019 Jun 18;17(24):5913-5915. doi: 10.1039/c9ob00961b.

PMID:
31165124
10.

Recent advances in the synthesis of gem-dimethylcyclobutane natural products.

Hancock EN, Wiest JM, Brown MK.

Nat Prod Rep. 2019 Oct 16;36(10):1383-1393. doi: 10.1039/c8np00083b.

PMID:
30855044
11.

Synthesis of Bisheteroarylalkanes by Heteroarylboration: Development and Application of a Pyridylidene-Copper Complex.

Huang Y, Brown MK.

Angew Chem Int Ed Engl. 2019 Apr 23;58(18):6048-6052. doi: 10.1002/anie.201902238. Epub 2019 Mar 27.

PMID:
30838739
12.

Impact of a Structured Weight Management Program on Worker Productivity.

Iyengar JJ, Miller NM, Ajluni N, Kraftson AT, Nay CK, Brown MK, Rothberg AE.

J Occup Environ Med. 2019 Feb;61(2):148-152. doi: 10.1097/JOM.0000000000001504.

PMID:
30730855
13.

Canvass: A Crowd-Sourced, Natural-Product Screening Library for Exploring Biological Space.

Kearney SE, Zahoránszky-Kőhalmi G, Brimacombe KR, Henderson MJ, Lynch C, Zhao T, Wan KK, Itkin Z, Dillon C, Shen M, Cheff DM, Lee TD, Bougie D, Cheng K, Coussens NP, Dorjsuren D, Eastman RT, Huang R, Iannotti MJ, Karavadhi S, Klumpp-Thomas C, Roth JS, Sakamuru S, Sun W, Titus SA, Yasgar A, Zhang YQ, Zhao J, Andrade RB, Brown MK, Burns NZ, Cha JK, Mevers EE, Clardy J, Clement JA, Crooks PA, Cuny GD, Ganor J, Moreno J, Morrill LA, Picazo E, Susick RB, Garg NK, Goess BC, Grossman RB, Hughes CC, Johnston JN, Joullie MM, Kinghorn AD, Kingston DGI, Krische MJ, Kwon O, Maimone TJ, Majumdar S, Maloney KN, Mohamed E, Murphy BT, Nagorny P, Olson DE, Overman LE, Brown LE, Snyder JK, Porco JA Jr, Rivas F, Ross SA, Sarpong R, Sharma I, Shaw JT, Xu Z, Shen B, Shi W, Stephenson CRJ, Verano AL, Tan DS, Tang Y, Taylor RE, Thomson RJ, Vosburg DA, Wu J, Wuest WM, Zakarian A, Zhang Y, Ren T, Zuo Z, Inglese J, Michael S, Simeonov A, Zheng W, Shinn P, Jadhav A, Boxer MB, Hall MD, Xia M, Guha R, Rohde JM.

ACS Cent Sci. 2018 Dec 26;4(12):1727-1741. doi: 10.1021/acscentsci.8b00747. Epub 2018 Dec 5.

14.

Catalyst-Controlled 1,2- and 1,1-Arylboration of α-Alkyl Alkenyl Arenes.

Bergmann AM, Dorn SK, Smith KB, Logan KM, Brown MK.

Angew Chem Int Ed Engl. 2019 Feb 4;58(6):1719-1723. doi: 10.1002/anie.201812533. Epub 2019 Jan 9.

15.

Allenoates in Enantioselective [2+2] Cycloadditions: From a Mechanistic Curiosity to a Stereospecific Transformation.

Wiest JM, Conner ML, Brown MK.

J Am Chem Soc. 2018 Nov 21;140(46):15943-15949. doi: 10.1021/jacs.8b10008. Epub 2018 Nov 5.

16.

Nickel-Catalyzed Stereoselective Diarylation of Alkenylarenes.

Gao P, Chen LA, Brown MK.

J Am Chem Soc. 2018 Aug 29;140(34):10653-10657. doi: 10.1021/jacs.8b05680. Epub 2018 Aug 20.

17.

Circadian Health and Light: A Report on the National Heart, Lung, and Blood Institute's Workshop.

Mason IC, Boubekri M, Figueiro MG, Hasler BP, Hattar S, Hill SM, Nelson RJ, Sharkey KM, Wright KP, Boyd WA, Brown MK, Laposky AD, Twery MJ, Zee PC.

J Biol Rhythms. 2018 Oct;33(5):451-457. doi: 10.1177/0748730418789506. Epub 2018 Jul 23.

18.

Early prediction of a significant patent ductus arteriosus in infants <32 weeks gestational age.

Katheria V, Poeltler DM, Brown MK, Hassen KO, Patel D, Rich W, Finer NN, Katheria AC.

J Neonatal Perinatal Med. 2018;11(3):265-271. doi: 10.3233/NPM-1771.

PMID:
29843271
19.

Impact of a neuro-intensive care service for newborns.

Harbert MJ, Sey R, Arnell K, Salinda L, Brown MK, Lazarus D, Poeltler DM, Wozniak PR, Rasmussen MR.

J Neonatal Perinatal Med. 2018;11(2):173-178. doi: 10.3233/NPM-181751.

PMID:
29843267
20.

Copper-catalyzed cross-coupling of aryl-, primary alkyl-, and secondary alkylboranes with heteroaryl bromides.

Bergmann AM, Oldham AM, You W, Brown MK.

Chem Commun (Camb). 2018 May 22;54(42):5381-5384. doi: 10.1039/c8cc03145b.

PMID:
29745398
21.

Copper-Catalyzed Heteroarylboration of 1,3-Dienes with 3-Bromopyridines: A cine Substitution.

Smith KB, Huang Y, Brown MK.

Angew Chem Int Ed Engl. 2018 May 22;57(21):6146-6149. doi: 10.1002/anie.201801139. Epub 2018 Apr 26.

22.

The Neu-Prem Trial: Neuromonitoring of Brains of Infants Born Preterm During Resuscitation-A Prospective Observational Cohort Study.

Katheria AC, Harbert MJ, Nagaraj SB, Arnell K, Poeltler DM, Brown MK, Rich W, Hassen KO, Finer N.

J Pediatr. 2018 Jul;198:209-213.e3. doi: 10.1016/j.jpeds.2018.02.065. Epub 2018 Apr 18.

PMID:
29680471
23.

Incidence of Hypocapnia, Hypercapnia, and Acidosis and the Associated Risk of Adverse Events in Preterm Neonates.

Brown MK, Poeltler DM, Hassen KO, Lazarus DV, Brown VK, Stout JJ, Rich WD, Katheria AC.

Respir Care. 2018 Aug;63(8):943-949. doi: 10.4187/respcare.05801. Epub 2018 Apr 3.

24.

Synthesis of (-)-Hebelophyllene E: An Entry to Geminal Dimethyl-Cyclobutanes by [2+2] Cycloaddition of Alkenes and Allenoates.

Wiest JM, Conner ML, Brown MK.

Angew Chem Int Ed Engl. 2018 Apr 16;57(17):4647-4651. doi: 10.1002/anie.201801110. Epub 2018 Mar 24.

25.

Nickel-Catalyzed Stereoselective Arylboration of Unactivated Alkenes.

Logan KM, Sardini SR, White SD, Brown MK.

J Am Chem Soc. 2018 Jan 10;140(1):159-162. doi: 10.1021/jacs.7b12160. Epub 2017 Dec 22.

26.

Design, optimisation and preliminary validation of a human specific loop-mediated amplification assay for the rapid detection of human DNA at forensic crime scenes.

Hird HJ, Brown MK.

Sci Justice. 2017 Nov;57(6):409-414. doi: 10.1016/j.scijus.2017.08.001. Epub 2017 Aug 3.

PMID:
29173453
27.

Synthesis of ent-[3]-Ladderanol: Development and Application of Intramolecular Chirality Transfer [2+2] Cycloadditions of Allenic Ketones and Alkenes.

Line NJ, Witherspoon BP, Hancock EN, Brown MK.

J Am Chem Soc. 2017 Oct 18;139(41):14392-14395. doi: 10.1021/jacs.7b09844. Epub 2017 Oct 6.

28.

Copper-Catalyzed Borylacylation of Activated Alkenes with Acid Chlorides.

Huang Y, Smith KB, Brown MK.

Angew Chem Int Ed Engl. 2017 Oct 16;56(43):13314-13318. doi: 10.1002/anie.201707323. Epub 2017 Sep 18.

29.

Catalyst Controlled Regiodivergent Arylboration of Dienes.

Sardini SR, Brown MK.

J Am Chem Soc. 2017 Jul 26;139(29):9823-9826. doi: 10.1021/jacs.7b05477. Epub 2017 Jul 12.

30.

Intramolecular Chirality Transfer [2 + 2] Cycloadditions of Allenoates and Alkenes.

Xu Y, Hong YJ, Tantillo DJ, Brown MK.

Org Lett. 2017 Jul 21;19(14):3703-3706. doi: 10.1021/acs.orglett.7b01420. Epub 2017 Jul 7.

31.

Regioselective Arylboration of Isoprene and Its Derivatives by Pd/Cu Cooperative Catalysis.

Smith KB, Brown MK.

J Am Chem Soc. 2017 Jun 14;139(23):7721-7724. doi: 10.1021/jacs.7b04024. Epub 2017 Jun 5.

32.

Reduced Sleep During Social Isolation Leads to Cellular Stress and Induction of the Unfolded Protein Response.

Brown MK, Strus E, Naidoo N.

Sleep. 2017 Jul 1;40(7). doi: 10.1093/sleep/zsx095.

33.

Delayed Cord Clamping in Newborns Born at Term at Risk for Resuscitation: A Feasibility Randomized Clinical Trial.

Katheria AC, Brown MK, Faksh A, Hassen KO, Rich W, Lazarus D, Steen J, Daneshmand SS, Finer NN.

J Pediatr. 2017 Aug;187:313-317.e1. doi: 10.1016/j.jpeds.2017.04.033. Epub 2017 May 16.

PMID:
28526223
34.

Hemodynamic effects of sodium bicarbonate administration.

Katheria AC, Brown MK, Hassan K, Poeltler DM, Patel DA, Brown VK, Sauberan JB.

J Perinatol. 2017 May;37(5):518-520. doi: 10.1038/jp.2016.258. Epub 2017 Feb 16.

PMID:
28206993
35.

Providing a Placental Transfusion in Newborns Who Need Resuscitation.

Katheria AC, Brown MK, Rich W, Arnell K.

Front Pediatr. 2017 Jan 25;5:1. doi: 10.3389/fped.2017.00001. eCollection 2017. Review.

36.

Catalytic Enantioselective Arylboration of Alkenylarenes.

Logan KM, Brown MK.

Angew Chem Int Ed Engl. 2017 Jan 16;56(3):851-855. doi: 10.1002/anie.201609844. Epub 2016 Dec 21.

37.

An unexpected Lewis acid catalyzed Diels-Alder cycloaddition of aryl allenes and acrylates.

Conner ML, Brown MK.

Tetrahedron. 2016 Jun 30;72(26):3759-3765. Epub 2016 Feb 18.

38.

Synthesis of 1,3-Substituted Cyclobutanes by Allenoate-Alkene [2 + 2] Cycloaddition.

Conner ML, Brown MK.

J Org Chem. 2016 Sep 2;81(17):8050-60. doi: 10.1021/acs.joc.6b01446. Epub 2016 Aug 25.

39.

Defining the Clinical Significance of Alloscardovia omnincolens in the Urinary Tract.

Brown MK, Forbes BA, Stitley K, Doern CD.

J Clin Microbiol. 2016 Jun;54(6):1552-1556. doi: 10.1128/JCM.03084-15. Epub 2016 Apr 6.

40.

Resistance of Colorimetric Carbon Dioxide Detectors Commonly Utilized in Neonates.

Brown MK, Lazarus DV, Gonzales SR, Rich WD, Wozniak MJ, Poeltler DM, Katheria AC.

Respir Care. 2016 Aug;61(8):1003-7. doi: 10.4187/respcare.04507. Epub 2016 Apr 5.

41.

Collaborative Total Synthesis: Routes to (±)-Hippolachnin A Enabled by Quadricyclane Cycloaddition and Late-Stage C-H Oxidation.

McCallum ME, Rasik CM, Wood JL, Brown MK.

J Am Chem Soc. 2016 Feb 24;138(7):2437-42. doi: 10.1021/jacs.5b13586. Epub 2016 Feb 9.

42.

Catalytic Enantioselective Diarylation of Alkenes.

You W, Brown MK.

J Am Chem Soc. 2015 Nov 25;137(46):14578-81. doi: 10.1021/jacs.5b10176. Epub 2015 Nov 13.

PMID:
26565926
43.

Lewis acid-promoted [2 + 2] cycloadditions of alkenes with aryl ketenes.

Rigsbee EM, Zhou C, Rasik CM, Spitz AZ, Nichols AJ, Brown MK.

Org Biomol Chem. 2016 Jun 28;14(24):5477-80. doi: 10.1039/c5ob01837d. Epub 2015 Sep 30.

44.

Cyclobutane and cyclobutene synthesis: catalytic enantioselective [2+2] cycloadditions.

Xu Y, Conner ML, Brown MK.

Angew Chem Int Ed Engl. 2015 Oct 5;54(41):11918-28. doi: 10.1002/anie.201502815. Epub 2015 Sep 2.

PMID:
26333192
45.

Catalytic enantioselective allenoate-alkene [2 + 2] cycloadditions.

Conner ML, Xu Y, Brown MK.

J Am Chem Soc. 2015 Mar 18;137(10):3482-5. doi: 10.1021/jacs.5b00563. Epub 2015 Mar 10.

PMID:
25756948
46.

Copper/palladium synergistic catalysis for the syn- and anti-selective carboboration of alkenes.

Logan KM, Smith KB, Brown MK.

Angew Chem Int Ed Engl. 2015 Apr 20;54(17):5228-31. doi: 10.1002/anie.201500396. Epub 2015 Feb 27.

PMID:
25727074
47.

Total synthesis of gracilioether F: development and application of lewis Acid promoted ketene-alkene [2+2] cycloadditions and late-stage C-H oxidation.

Rasik CM, Brown MK.

Angew Chem Int Ed Engl. 2014 Dec 22;53(52):14522-6. doi: 10.1002/anie.201408055. Epub 2014 Oct 30.

PMID:
25359632
48.

Diarylation of alkenes by a Cu-catalyzed migratory insertion/cross-coupling cascade.

You W, Brown MK.

J Am Chem Soc. 2014 Oct 22;136(42):14730-3. doi: 10.1021/ja509056j. Epub 2014 Oct 10.

PMID:
25303225
49.

Origins of diastereoselectivity in Lewis acid promoted ketene-alkene [2 + 2] cycloadditions.

Rasik CM, Hong YJ, Tantillo DJ, Brown MK.

Org Lett. 2014 Oct 3;16(19):5168-71. doi: 10.1021/ol5025184. Epub 2014 Sep 17.

PMID:
25230201
50.

Alkene carboboration enabled by synergistic catalysis.

Smith KB, Logan KM, You W, Brown MK.

Chemistry. 2014 Sep 15;20(38):12032-6. doi: 10.1002/chem.201404310. Epub 2014 Aug 11.

PMID:
25113669

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