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Angew Chem Int Ed Engl. 2009;48(8):1479-83. doi: 10.1002/anie.200804927.

Clean absorption-mode NMR data acquisition.

Author information

1
Department of Chemistry, State University of New York at Buffalo, Buffalo, New York 14260, USA.

Abstract

A new acquisition: Based on "phase-shifted mirrored sampling" (PMS) of indirect evolution periods of multi-dimensional experiments, new acquisition schemes eliminate, without application of a phase correction, dispersive signal components that exacerbate peak identification and shift peak maxima. The resulting enhanced resolution is of particular value for systems with high chemical shift degeneracy.

PMID:
19140147
PMCID:
PMC3018340
DOI:
10.1002/anie.200804927
[Indexed for MEDLINE]
Free PMC Article

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