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Chemical synthesis of benzamide adenine dinucleotide: inhibition of inosine monophosphate dehydrogenase (types I and II).
Zatorski A, Watanabe KA, Carr SF, Goldstein BM, Pankiewicz KW. Zatorski A, et al. J Med Chem. 1996 Jun 7;39(12):2422-6. doi: 10.1021/jm9601415. J Med Chem. 1996. PMID: 8691436
Reaction of 6 with 2-cyanoethyl N,N-diisopropylchlorophosphoramidite followed by 2-cyanoethanol/tetrazole treatment and oxidation with tert-butyl peroxide gave a 1:1 mixture of the desired 5'-O-bis(2-cyanoethyl) phosphate 9 and the chloro derivative 7. ...
Reaction of 6 with 2-cyanoethyl N,N-diisopropylchlorophosphoramidite followed by 2-cyanoethanol/tetrazole treatment and oxidat …
The reactivity of phosphomono-and phosphodiester groups in oligonucleotides.
Knorre DG, Zrytova VF, Lebedev AV, Khalimskaya LM, Sheshogova EA. Knorre DG, et al. Nucleic Acids Res. 1978 Apr;5(4):1253-72. doi: 10.1093/nar/5.4.1253. Nucleic Acids Res. 1978. PMID: 206874 Free PMC article.
The rate constants were estimated by phosphorus NMR spectroscopy for the reactions of alcohols (Tr-dT, 2-cyanoethanol) in pyridine with the main types of the reactive phosphorylating intermediates formed by treatment of pdT-Ac, pdTpdT-Ac, Tr-dTpdT-Ac, Tr-dTpdTpdT-Ac …
The rate constants were estimated by phosphorus NMR spectroscopy for the reactions of alcohols (Tr-dT, 2-cyanoethanol) in pyri …