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J Mass Spectrom. 1997 Jan;32(1):64-70.

High-performance liquid chromatography/NMR spectrometry/mass spectrometry: further advances in hyphenated technology.

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Pfizer Central Research, Sandwich, Kent, UK.


The earlier use of combined liquid chromatography/NMR spectrometry/mass spectrometry (LC/NMR/MS) involved the use of a particle beam interface. This paper describes further developments of this hyphenated technology, in particular the incorporation of an electrospray interface into the LC/NMR/MS system. This improved LC/NMR/MS system was designed for the support of a combinatorial library program. The power of this technique is demonstrated in the successful structural elucidation of each compound in a mixture of commercially available peptides.

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