Rapid and solvent-saving liquefaction of woody biomass using microwave-ultrasonic assisted technology

Bioresour Technol. 2016 Jan:199:423-426. doi: 10.1016/j.biortech.2015.09.048. Epub 2015 Sep 18.

Abstract

A novel process to rapidly liquefy sawdust using reduced quantities of solvent, was successfully carried out via microwave-ultrasonic assisted technology (MUAT) in a sulphuric acid/polyethylene glycol 400-glycerol catalytic system. The influences of some key parameters on the liquefaction yield were investigated. The results showed that compared with traditional liquefaction, the introduction of MUAT allowed the solvent dosage to be halved and shortened the liquefaction time from 60 to 20 min. The liquefaction yield reached 91% under the optimal conditions. However, the influence on the yield of some parameters such as catalyst concentration, was similar to that of traditional liquefaction, indicating that the application of MUAT possibly only intensified heat and mass transfer rather than altering either the degradation mechanism or pathway. The introduction of MUAT as a process intensification technology has good industrial application potential for woody biomass liquefaction.

Keywords: Biomass; Liquefaction; Microwave; Ultrasonic wave.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Biofuels
  • Biomass
  • Biotechnology / methods
  • Catalysis
  • Glycerol / chemistry
  • Hot Temperature
  • Industrial Waste*
  • Microwaves*
  • Polyethylene Glycols / chemistry
  • Refuse Disposal / methods
  • Solvents / chemistry
  • Sulfuric Acids / chemistry
  • Ultrasonics / methods*
  • Wood / chemistry*

Substances

  • Biofuels
  • Industrial Waste
  • Solvents
  • Sulfuric Acids
  • Polyethylene Glycols
  • polyethylene glycol 400
  • sulfuric acid
  • Glycerol