Effect of post-curing treatment on mechanical properties of composite resins

Acta Odontol Latinoam. 2014;27(2):72-6. doi: 10.1590/S1852-48342014000200005.

Abstract

The aim of this study is to assess the effect of additional curing procedures on the flexural strength and modulus of elasticity of indirect and direct composite materials. Twenty-four rectangular prism-shaped 2 mm x 2 mm x 25 mm samples of Belleglass, Premisa (Kerr), Adoro and Heliomolar (Ivoclar Vivadent) were prepared. Each composite was packed in an ad-hoc stainless steel device with a TeflonR instrument. A mylar strip and a glass slab were placed on top to obtain a flat surface. Polymerization was activated for 20 seconds with a halogen unit (Astralis 10, Ivoclar - Vivadent) with soft start regime and an output with a 350 to 1200 mw/cm2 range at four different points according to the diameter of the end of the guide. The specimens obtained were then randomly divided into two different groups: with and without additional treatment. In the group with additional treatment, the samples adorro were submitted to 25 minutes in Lumamat 100 (Ivoclar Vivadent) and the rest to 20 minutes in BelleGlass HP (Kerr). After the curing procedures, all samples were treated with sandpapers of decreasing grain size under water flow, and stored in distilled water for 24 h. Flexural strength was measured according to the ISO 404920 recommendations and elastic modulus was determined following the procedures of ANSI/ADA standard No. 27. Statistical differences were found among the different materials and curing procedures employed (P<0.01). The elastic modulus was significantly higher after the additional curing treatment for all materials except Premisa. Further work is needed to determine the association between the actual monomers present in the matrix and the effect of additional curing processes on the mechanical properties of both direct and indirect composites, and its clinical relevance.

Publication types

  • Comparative Study
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Acrylic Resins / chemistry
  • Acrylic Resins / radiation effects
  • Composite Resins / chemistry*
  • Composite Resins / radiation effects
  • Curing Lights, Dental / classification
  • Dental Materials / chemistry*
  • Dental Materials / radiation effects
  • Dental Polishing / instrumentation
  • Elastic Modulus
  • Humans
  • Light-Curing of Dental Adhesives / instrumentation
  • Light-Curing of Dental Adhesives / methods
  • Materials Testing
  • Mechanical Phenomena
  • Methacrylates / chemistry
  • Methacrylates / radiation effects
  • Pliability
  • Polymerization
  • Polyurethanes / chemistry
  • Polyurethanes / radiation effects
  • Radiation Dosage
  • Random Allocation
  • Stress, Mechanical
  • Surface Properties
  • Time Factors
  • Water / chemistry

Substances

  • Acrylic Resins
  • Composite Resins
  • Dental Materials
  • Heliomolar
  • Methacrylates
  • Polyurethanes
  • belleGlass
  • premise composite resin
  • Water