Development of a method for measuring the density of liquid sulfur at high pressures using the falling-sphere technique

Rev Sci Instrum. 2012 Oct;83(10):103908. doi: 10.1063/1.4757570.

Abstract

We describe a new method for the in situ measurement of the density of a liquid at high pressure and high temperature using the falling-sphere technique. Combining synchrotron radiation X-ray radiography with a large-volume press, the newly developed falling-sphere method enables the determination of the density of a liquid at high pressure and high temperature based on Stokes' flow law. We applied this method to liquid sulfur and successfully obtained the density at pressures up to 9 GPa. Our method could be used for the determination of the densities of other liquid materials at higher static pressures than are currently possible.