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Inorg Chem. 2012 Aug 6;51(15):7945-7. doi: 10.1021/ic301422x. Epub 2012 Jul 12.

Solvent-mediated room temperature synthesis of highly crystalline Cu9S5 (Cu1.8S), CuSe, PbS, and PbSe from their elements.

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1
Materials Chemistry Group, Department of Chemistry, University of Delhi, Delhi 110007, India.

Abstract

Highly crystalline Cu(9)S(5) (Cu(1.8)S), CuSe, PbS, and PbSe are obtained by reacting the elements in 2-mercaptoethanol as the solvent for 24 h at room temperature. The elemental reactions of copper and lead with sulfur in ethylene glycol were successful, yielding CuS and PbS, respectively. Metal sulfide formation was not observed using dimercaptoethane.

PMID:
22789059
DOI:
10.1021/ic301422x
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