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Chem Commun (Camb). 2012 Feb 28;48(18):2442-4. doi: 10.1039/c2cc15670a. Epub 2012 Jan 23.

First domino radical cyclisation/Smiles rearrangement combination.

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1
Institut de Chimie Moléculaire de Reims, UMR CNRS 6229, Université de Reims-Champagne-Ardenne, Faculté de Pharmacie, 51 rue Cognacq-Jay, F-51096 Reims, Cedex, France.

Abstract

An unprecedented domino radical cyclisation-Smiles rearrangement process affording 3-(2'-aryl-N-methyl acetamido)indolin-2-ones is presented. Experimental rationalisation of this approach and description of an unexpected tricyclic core are also handled.

PMID:
22266569
DOI:
10.1039/c2cc15670a
[Indexed for MEDLINE]
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