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Chem Commun (Camb). 2012 Feb 1;48(10):1526-8. doi: 10.1039/c1cc14724b. Epub 2011 Sep 5.

Sulfo-click reaction via in situ generated thioacids and its application in kinetic target-guided synthesis.

Author information

1
Department of Chemistry, University of South Florida, 4202 E Fowler Ave., Tampa, FL 33620, USA.

Abstract

Herein, we describe a practical, one-pot variant of the sulfo-click reaction, in which 9-fluorenylmethyl-protected thioesters are rapidly deprotected and reacted further with sulfonylazides to give N-acyl sulfonamides.

PMID:
21892513
DOI:
10.1039/c1cc14724b
[Indexed for MEDLINE]

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