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Dalton Trans. 2010 Feb 28;39(8):1985-8. doi: 10.1039/b919177a. Epub 2009 Dec 23.

Solvothermal synthesis and magnetic properties of 3D flower-like NiHPO(3).H(2)O superstructures.

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College of Chemistry, Northeast Normal University, Changchun, 130024, China.


A self-assembled three-dimensional (3D) flower-like NiHPO(3).H(2)O micro/nanocomposite structure has been successfully synthesized for the first time by a simple solvothermal method, employing Na(6)P(6)O(18) as the phosphor source without the assistance of any template or surfactant. The as-obtained product was characterized by X-ray powder diffraction, scanning electron microscopy and transmission electron microscopy. The formation mechanism was proposed based on the evolution of this morphology as a function of solvothermal time. Some factors influencing the morphology of the NiHPO(3).H(2)O flower-like micro/nanocomposite structures were systematically investigated. The magnetic measurements demonstrated that the flower-like 3D superstructures exhibit ferromagnetic property.


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