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Org Lett. 2009 Jul 16;11(14):3048-51. doi: 10.1021/ol901086f.

Multistep one-pot Wittig/Nazarov reaction for construction of cyclopentenone with diazo compounds and acid chlorides.

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1
State Key Laboratory of Organometallic Chemistry, Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences, 345 Lingling Lu, Shanghai 200032, China.

Abstract

A facile multistep one-pot synthesis of single or fused cyclopentenones has been developed. The sequence involves a transition metal-catalyzed ylide formation/Wittig Olefination/Nazarov Cyclization.

PMID:
19522525
DOI:
10.1021/ol901086f
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