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Bioorg Med Chem Lett. 2009 Jul 15;19(14):3848-51. doi: 10.1016/j.bmcl.2009.03.148. Epub 2009 Apr 5.

Hypervalent iodine-catalyzed oxylactonization of ketocarboxylic acids to ketolactones.

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  • 1Graduate School of Engineering, Nagoya University, Chikusa, Nagoya 464-8603, Japan.

Abstract

The hypervalent iodine-catalyzed oxylactonization of ketocarboxylic acids to ketolactones was achieved in the presence of iodobenzene (10 mol%), p-toluenesulfonic acid monohydrate (20 mol%) and meta-chloroperbenzoic acid as a stoichiometric co-oxidant.

PMID:
19376702
DOI:
10.1016/j.bmcl.2009.03.148
[PubMed - indexed for MEDLINE]
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