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Rev Sci Instrum. 2008 Aug;79(8):083901. doi: 10.1063/1.2957611.

Indirect measurement of the magnetocaloric effect using a novel differential scanning calorimeter with magnetic field.

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1
Fuel Cells and Solid State Chemistry Department, Riso DTU, Technical University of Denmark, DK-4000 Roskilde, Denmark.

Abstract

A simple and high-sensitivity differential scanning calorimeter (DSC) unit operating under magnetic field has been built for indirect determination of the magnetocaloric effect. The principle of the measuring unit in the calorimeter is based on Peltier elements as heat flow sensors. The high sensitivity of the apparatus combined with a suitable calibration procedure allows very fast and accurate heat capacity measurements under magnetic field to be made. The device was validated from heat capacity measurements for the typical DSC reference material gallium (Ga) and a La(0.67)Ca(0.33)MnO(3) manganite system and the results were highly consistent with previous reported data for these materials. The DSC has a working range from 200 to 340 K and has been tested in magnetic fields reaching 1.8 T. The signal-to-noise ratio is in the range of 10(2)-10(3) for the described experiments. Finally the results have been compared to results from a Quantum Design(R) physical properties measuring system. The configuration of the system also has the advantage of being able to operate with other types of magnets, e.g., permanent magnets or superconducting coils, as well as the ability to be expanded to a wider temperature range.

PMID:
19044358
DOI:
10.1063/1.2957611
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