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J Am Chem Soc. 2008 Nov 12;130(45):14910-1. doi: 10.1021/ja804448p. Epub 2008 Oct 16.

Azidation of silicon(111) surfaces.

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  • 1Division of Chemistry and Chemical Engineering, Noyes Laboratory, 127-72, Kavli Nanoscience Institute, California Institute of Technology, Pasadena, California 91125

Abstract

A two-step chlorination/azidation process was reported to prepare azide-modified silicon(111) surfaces. XPS and IR analyses show the covalent bonding of azide with silicon. In combination with scanning tunneling microscopy and spectroscopy analyses, different kinetic rates, azide coverages, and surface-area distributions were derived depending on the azidation solvent.

PMID:
18922002
DOI:
10.1021/ja804448p
[PubMed]
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