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Carbohydr Res. 2008 May 5;343(6):1114-9. doi: 10.1016/j.carres.2008.01.043. Epub 2008 Feb 7.

Development of a 1H NMR structural-reporter-group concept for the primary structural characterisation of alpha-D-glucans.

Author information

1
Bijvoet Center, Department of Bio-Organic Chemistry, Utrecht University, Padualaan 8, 3584 CH Utrecht, The Netherlands.

Abstract

An NMR study of proton chemical shift patterns of known linear alpha-D-glucopyranose di- and trisaccharide structures was carried out. Chemical shift patterns for (alpha1-->2)-, (alpha1-->3)-, (alpha1-->4)- and (alpha1-->6)-linked D-glucose residues were analysed and compared to literature data. Using these data, a 1H NMR structural-reporter-group concept was formulated to function as a tool in the structural analysis of alpha-D-glucans.

PMID:
18314096
DOI:
10.1016/j.carres.2008.01.043
[Indexed for MEDLINE]

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