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Arch Pharm Res. 2008 Jan;31(1):6-9.

Application of coupling reaction between lithiated toluamide and benzonitrile for the synthesis of phenolic benzo[c]phenanthridine alkaloid, oxyterihanine.

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1
College of Pharmacy, Research Institute of Drug Development, Chonnam National University, Gwangju 500-757, Korea.

Abstract

The total synthesis of the natural phenolic benzo[c]phenanthridine alkaloid, oxyterihanine, was accomplished via substituted 3-arylisoquinoline intermediate. The key reaction was a coupling between the o-toluamide 4 and the benzonitrile 5.

PMID:
18277600
[Indexed for MEDLINE]
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