Format

Send to

Choose Destination
See comment in PubMed Commons below
J Chromatogr A. 2002 Sep 13;970(1-2):225-34.

Characterisation of lavender essential oils by using gas chromatography-mass spectrometry with correlation of linear retention indices and comparison with comprehensive two-dimensional gas chromatography.

Author information

1
Australian Centre for Research on Separation Science, Department of Applied Chemistry, RMIT University, Melbourne, Victoria.

Abstract

Nine samples of lavender essential oil were analysed by GC-MS using low-polarity and polar capillary columns. Linear retention indices (LRI) were calculated for each component detected. Characterisation of the individual components making up the oils was performed with the use of an mass spectrometry (MS) library developed in-house. The MS library was designed to incorporate the chromatographic data in the form of linear retention indices. The MS search routine used linear retention indices as a post-search filter and identification of the "unknowns" was made more reliable as this approach provided two independent parameters on which the identification was based. Around 70% of the total number of components in each sample were reliably characterised. A total of 85 components were identified. Semi-quantitative analysis of the same nine samples was performed by gas chromatography (GC) with flame ionisation detection (FID). The identified components accounted for more than 95% of each oil. By comparing the GC-MS results with the results from the GCxGC-FID analysis of a lavender essential oil, many more components could be found within the two-dimensional separation space.

PMID:
12350096
[Indexed for MEDLINE]
PubMed Commons home

PubMed Commons

0 comments
How to join PubMed Commons

    Supplemental Content

    Loading ...
    Support Center