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Acta Crystallogr D Biol Crystallogr. 2001 May;57(Pt 5):755-8. Epub 2001 Apr 24.

Structure of the macrocycle thiostrepton solved using the anomalous dispersion contribution of sulfur.

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1
The Wellcome Trust Biocentre, University of Dundee, Dundee DD1 5EH, Scotland, UK.

Abstract

The structure of a tetragonal crystal form of thiostrepton has been solved using the anomalous dispersive effects of five S atoms from high-redundancy data collected to 1.33 A resolution at the Cu Kalpha wavelength. Data measured to 1.02 A resolution with a synchrotron source were used for refinement. Details of the molecular structure, intramolecular and intermolecular interactions are given.

PMID:
11320328
[Indexed for MEDLINE]

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