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Carbohydr Res. 2000 Sep 22;328(3):431-4.

A convenient synthesis of glycosyl chlorides from sugar hemiacetals using triphosgene as the chlorine source.

Author information

1
Department of Chemistry, Youngstown State University, OH 44555-3663, USA.

Abstract

Treating partially protected sugar hemiacetals with triphosgene in THF results in the formation of glycosyl chlorides. The method is compatible with acid-sensitive isopropylidene protecting groups in the hemiacetal substrates.

PMID:
11072851
[Indexed for MEDLINE]

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