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Org Lett. 1999 Dec 2;1(11):1811-4.

Solid-phase oligosaccharide synthesis: preparation of complex structures using a novel linker and different glycosylating agents.

Author information

1
Department of Chemistry, Massachusetts Institute of Technology, Cambridge 02139, USA.

Abstract

[formula: see text] A beta-(1-->4)-linked trisaccharide was prepared in 53% yield on a polymer support using glycosyl phosphates and released by cross-metathesis of a novel linker to reveal the anomeric n-pentenyl glycoside. Heptasaccharide 33 was prepared in 9% yield in 14 steps.

PMID:
10836038
DOI:
10.1021/ol991071+
[Indexed for MEDLINE]

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