Separation and identification of perchlorinated polycyclic aromatic hydrocarbons by high-performance liquid chromatography and ultraviolet absorption spectroscopy

S Y Xie; R B Huang; L S Zheng

doi:10.1016/s0021-9673(99)00956-5

Separation and identification of perchlorinated polycyclic aromatic hydrocarbons by high-performance liquid chromatography and ultraviolet absorption spectroscopy

J Chromatogr A. 1999 Dec 9;864(1):173-7. doi: 10.1016/s0021-9673(99)00956-5.

Authors

S Y Xie¹, R B Huang, L S Zheng

Affiliation

¹ State Key Laboratory for Physical Chemistry of Solid Surface, Department of Chemistry, Xiamen University, China.

PMID: 10630882
DOI: 10.1016/s0021-9673(99)00956-5

Abstract

High-performance liquid chromatography (HPLC) was coupled with ultraviolet absorption spectroscopy (UV) for the simultaneous separation and identification of a series of perchlorinated polycyclic aromatic hydrocarbons, such as perchlorobenzene (C6Cl6), perchloronaphthalene (C10Cl8), perchlorobiphenyl (C12Cl10), perchloroanthracene (C14Cl10), perchlorophenanthrene (C14C10), perchloroacenaphthylene (C12Cl8), perchloropyrene (C16Cl10) and perchlorofluoranthene (C16Cl10). HPLC was performed on an ODS column using methanol-hexane (80:20) as mobile phase at a flow-rate of 1.0 ml/min. UV absorption spectra of the elutes were detected in the region of 210-350 nm.

Publication types

Research Support, Non-U.S. Gov't

MeSH terms

Chromatography, High Pressure Liquid / methods*
Hydrocarbons, Chlorinated / analysis*
Hydrocarbons, Chlorinated / isolation & purification*
Polycyclic Aromatic Hydrocarbons / analysis*
Polycyclic Aromatic Hydrocarbons / isolation & purification*
Spectrophotometry, Ultraviolet*

Substances

Hydrocarbons, Chlorinated
Polycyclic Aromatic Hydrocarbons