Synthesis and characterization of d5 -barbarin for use in barbarin-related research.
Kudrimoti S, Machin J, Arojojoye AS, Awuah SG, Eisenberg R, Fenger C, Maylin G, Lehner AF, Tobin T.
Kudrimoti S, et al.
Drug Test Anal. 2023 Jan;15(1):42-46. doi: 10.1002/dta.3357. Epub 2022 Aug 23.
Drug Test Anal. 2023.
PMID: 35975356
Free PMC article.
D(5) -barbarin synthesis commenced with production of d(5) -2-oxo-2-phenylacetaldehyde oxime (d(5) -oxime) from d(5) -acetophenone via butylnitrite in an ethoxide/ethanol solution. This d(5) -oxime was then reduced with lithium aluminum hydride (LiAlH(4) ) to produc …
D(5) -barbarin synthesis commenced with production of d(5) -2-oxo-2-phenylacetaldehyde oxime (d(5) -oxime) from d(5) -acetophenone via butyl …