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Appl Radiat Isot. 2014 Jun;88:74-7. doi: 10.1016/j.apradiso.2013.12.020. Epub 2014 Jan 25.

(10)B-NMR determination of (10)B-BPA, (10)B-BPA-fructose complex and total (10)B in blood for BNCT.

Author information

  • 1Department of Chemistry, Faculty of Science, Shinshu University, Asahi, Matsumoto, Nagano 390-8621, Japan. Electronic address: yoshino@shinshu-u.ac.jp.
  • 2Department of Chemistry, Faculty of Science, Shinshu University, Asahi, Matsumoto, Nagano 390-8621, Japan.

Abstract

First spontaneous, noninvasive determination method of (10)B-BPA, (10)B-BPA-fructose complex, and total (10)B in blood is described. (10)B-NMR measurement with 100,000 FT accumulation enables us to obtain the result within 100min/sample. The detection limits for the simultaneous analysis were 3ppm, 3ppm and 6ppm for (10)B-BPA, (10)B-BPA-fructose complex and total (10)B respectively in this study. By this method, we can actually discuss behavior of the (10)B-BPA-fructose complex in blood.

Copyright © 2014 Elsevier Ltd. All rights reserved.

KEYWORDS:

(10)B-NMR; (10)B-analysis; BNCT; BPA; BPA–fructose complex; Red cell components (RCC)

PMID:
24530317
[PubMed - indexed for MEDLINE]
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