Send to:

Choose Destination
See comment in PubMed Commons below
Chem Commun (Camb). 2014 Mar 7;50(19):2512-4. doi: 10.1039/c3cc49659g. Epub 2014 Jan 24.

Diastereomeric ratio determination by high sensitivity band-selective pure shift NMR spectroscopy.

Author information

  • 1School of Chemistry, University of Manchester, Oxford Road, Manchester, M13 9PL, UK.


An NMR method is reported that allows diastereomeric ratios to be determined even in crowded spectra or where chemical shift differences are small compared to multiplet widths. Band-selective pure shift NMR collapses multiplets to singlets, greatly improving spectral resolution while largely retaining, or even enhancing, signal-to-noise ratio.

[PubMed - indexed for MEDLINE]
PubMed Commons home

PubMed Commons

How to join PubMed Commons

    Supplemental Content

    Full text links

    Icon for Royal Society of Chemistry
    Loading ...
    Write to the Help Desk