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Org Lett. 2013 Jul 19;15(14):3722-5. doi: 10.1021/ol401593a. Epub 2013 Jul 3.

Iridium-catalyzed enantioselective hydrogenation of α,β-unsaturated carboxylic acids with tetrasubstituted olefins.

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  • 1State Key Laboratory and Institute of Elemento-organic Chemistry, Nankai University, Tianjin 300071, China.

Abstract

A highly efficient asymmetric hydrogenation of α,β-unsaturated carboxylic acids with tetrasubstituted olefin catalyzed by chiral spiro iridium complexes has been developed for the preparation of chiral α-substituted carboxylic acids in excellent enantioselectivities (up to 99% ee).

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