Determination of U and Th α-emitters in NORM samples through extraction chromatography by using new and recycled UTEVA resins

N Casacuberta; M Lehritani; J Mantero; P Masqué; J Garcia-Orellana; R Garcia-Tenorio

doi:10.1016/j.apradiso.2011.11.063

Determination of U and Th α-emitters in NORM samples through extraction chromatography by using new and recycled UTEVA resins

Appl Radiat Isot. 2012 Apr;70(4):568-73. doi: 10.1016/j.apradiso.2011.11.063. Epub 2011 Dec 16.

Authors

N Casacuberta¹, M Lehritani, J Mantero, P Masqué, J Garcia-Orellana, R Garcia-Tenorio

Affiliation

¹ Institut de Ciència i Tecnologia Ambientals-Departament de Física, Universitat Autònoma de Barcelona, 08193 Bellaterra, Spain. Nuria.Casacuberta@uab.es

PMID: 22197462
DOI: 10.1016/j.apradiso.2011.11.063

Abstract

This manuscript describes a protocol for the determination of U and Th isotopes via alpha spectrometry in NORM samples containing high concentrations of these radionuclides, up to kBq kg(-1). This technique is based on extraction chromatography with UTEVA (Triskem Int.) resins and it has been tested using both NORM samples from a phosphate industry and reference materials. The results proved that this method is highly optimized in terms of accuracy and precision when dealing with NORM samples. Recycling of UTEVA columns was also checked using NORM samples and successful results were obtained for both U and Th isotopes, thus proving the feasibility of re-using these type of columns.