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    J Org Chem. 2009 Nov 20;74(22):8626-37.

    Quantum-mechanical study of 10-R-9-borabicyclo[3.3.2]decane alkene hydroboration.

    Ess DH, Kister J, Chen M, Roush WR.

    Department of Chemistry, The Scripps Research Institute, Scripps Florida, Jupiter, Florida 33458, USA. daniel@scripps.edu

    Density functional theory and correlated ab initio quantum mechanical methods were used to locate and analyze alkene hydroboration transition structures for 10-R-9-borabicyclo[3.3.2]decane reagents. Transition-state ensembles quantitatively modeled enantioselectivity for hydroboration of cis-, trans-, and gem-disubstituted alkenes in excellent agreement with experiment. The 10-R group and borabicyclo[3.3.2]decane ring conformation effects were analyzed to understand the origin of asymmetric selectivity.

    PMID: 19824624 [PubMed - in process]

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