Synthesis of Beta/MCM-41 composite molecular sieve with high hydrothermal stability in static and stirred condition

Haiyan Xu; Jingqi Guan; Shujie Wu; Qiubin Kan

doi:10.1016/j.jcis.2008.10.002

Synthesis of Beta/MCM-41 composite molecular sieve with high hydrothermal stability in static and stirred condition

J Colloid Interface Sci. 2009 Jan 15;329(2):346-50. doi: 10.1016/j.jcis.2008.10.002. Epub 2008 Oct 8.

Authors

Haiyan Xu¹, Jingqi Guan, Shujie Wu, Qiubin Kan

Affiliation

¹ College of Chemistry, Jilin University, Changchun, 130023, PR China.

PMID: 18951553
DOI: 10.1016/j.jcis.2008.10.002

Abstract

Beta/MCM-41 micro/mesoporous composite materials have been prepared through assembly of zeolite Beta nanoclusters and their hydrolysis products in the presence of CTAB under static or stirred conditions. The resulting materials were characterized by powder XRD, TEM and nitrogen adsorption-desorption. Hydrothermal stability of the obtained Beta/MCM-41 composites was evaluated by boiling in distilled water for different periods of time under refluxing. All materials exhibit very high hydrothermal stability.