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Anal Biochem. 2008 May 15;376(2):283-5. doi: 10.1016/j.ab.2008.01.027. Epub 2008 Jan 31.

Analysis of trimethyl carboxyphosphate by gas chromatography-mass spectrometry.

Author information

  • 1School of Biomedical, Biomolecular and Chemical Sciences, The University of Western Australia, Crawley, WA 6009, Australia. mjm@cyllene.uwa.edu.au

Abstract

Analysis of trimethyl carboxyphosphate samples by gas chromatography-mass spectrometry, using typical conditions resulted in significant decomposition of the analyte. Optimization of injection conditions, including conditioning of the injection port liner, produced a dramatic increase in observed peak areas and afforded an effective method for detection of trimethyl carboxyphosphate at the <1 microg mL(-1) level.

PMID:
18294947
[PubMed - indexed for MEDLINE]
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