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Chem Commun (Camb). 2006 Apr 7;(13):1398-400. Epub 2006 Mar 3.

Iron nanoparticles in the coupling of alkyl halides with aryl Grignard reagents.

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  • 1School of Chemistry, University of Bristol, Cantock's Close, Bristol, UKBS8 1TS. r.bedford@bristol.ac.uk

Abstract

Iron nanoparticles, either formed in situ stabilized by 1,6-bis(diphenylphosphino)hexane or polyethylene glycol (PEG), or preformed stabilized by PEG, are excellent catalysts for the cross-coupling of aryl Grignard reagents with primary and secondary alkyl halides bearing beta-hydrogens and they also prove effective in a tandem cyclization/cross-coupling reaction.

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