J Chromatogr. 1992 Mar 20;595(1-2):259-67.

Determination of alpha- and beta-zearalenol and zearalenone in cereals by gas chromatography with ion-trap detection.

Source

Institute of Animal Nutrition, University of Hohenheim, Stuttgart, Germany.

Abstract

A method for determination of estrogenic mycotoxins, alpha- and beta-zearalenol and zearalenone, in cereals (wheat, barley, oats, corn) is described. After extraction with ethylacetate, clean-up involved a base treatment and partition with water; derivatization was by trimethylsilylation. For quantitation and confirmation a capillary gas chromatograph combined with a selective mass detector (ion trap), working in the electron impact-mode was used. The detection limit for the complete method is 1 microgram/kg for each of the three mycotoxins in full scan. Recoveries from spiked cereals were 82-86%.

PMID:: 1533645; [PubMed - indexed for MEDLINE]

MeSH Terms, Substances

MeSH Terms

Substances

LinkOut - more resources

Full Text Sources

EBSCO

Molecular Biology Databases

ZEARALENONE - HSDB

Supplemental Content

Save items

Related citations in PubMed

[Determination of zearalenone and its metabolites in grains by capillary electrophoresis]. [Sichuan Da Xue Xue Bao Yi Xue ...]
[Determination of zearalenone and its metabolites in grains by capillary electrophoresis].
Zeng H, Li Y, Jin J, Sun H. Sichuan Da Xue Xue Bao Yi Xue Ban. 2003 Apr; 34(2):333-6.
Liquid chromatographic determination of zearalenone and zearalenol in animal feeds and grains, using fluorescence detection. [J Assoc Off Anal Chem. 1986]
Liquid chromatographic determination of zearalenone and zearalenol in animal feeds and grains, using fluorescence detection.
Bagneris RW, Gaul JA, Ware GM. J Assoc Off Anal Chem. 1986 Sep-Oct; 69(5):894-8.
Rapid, sensitive liquid chromatographic method for determination of zearalenone and alpha- and beta-zearalenol in wheat. [J Assoc Off Anal Chem. 1984]
Rapid, sensitive liquid chromatographic method for determination of zearalenone and alpha- and beta-zearalenol in wheat.
Trenholm HL, Warner RM, Fitzpatrick DW. J Assoc Off Anal Chem. 1984 Sep-Oct; 67(5):968-72.
A rapid method for simultaneous determination of zearalenone, α-zearalenol, β-zearalenol, zearalanone, α-zearalanol and β-zearalanol in traditional Chinese medicines by ultra-high-performance liquid chromatography-tandem mass spectrometry. [J Chromatogr B Analyt Technol ...]
A rapid method for simultaneous determination of zearalenone, α-zearalenol, β-zearalenol, zearalanone, α-zearalanol and β-zearalanol in traditional Chinese medicines by ultra-high-performance liquid chromatography-tandem mass spectrometry.
Han Z, Ren Y, Zhou H, Luan L, Cai Z, Wu Y. J Chromatogr B Analyt Technol Biomed Life Sci. 2011 Feb 15; 879(5-6):411-20. Epub 2010 Dec 31.
Rapid thin layer chromatographic method for determination of zearalenone and zearalenol in grains and animal feeds. [J Assoc Off Anal Chem. 1984]
Rapid thin layer chromatographic method for determination of zearalenone and zearalenol in grains and animal feeds.
Swanson SP, Corley RA, White DG, Buck WB. J Assoc Off Anal Chem. 1984 May-Jun; 67(3):580-2.

See reviews... See all...

Related information

Related Citations
Calculated set of PubMed citations closely related to the selected article(s) retrieved using a word weight algorithm. Related articles are displayed in ranked order from most to least relevant, with the “linked from” citation displayed first.
Compound (MeSH Keyword)
PubChem chemical compound records that are classified under the same Medical Subject Headings (MeSH) controlled vocabulary as the current articles.
Substance (MeSH Keyword)
PubChem chemical substance (submitted) records that are classified under the same Medical Subject Headings (MeSH) controlled vocabulary as the current articles.

Recent activity

Clear Turn Off Turn On

Determination of alpha- and beta-zearalenol and zearalenone in cereals by gas ch...
Determination of alpha- and beta-zearalenol and zearalenone in cereals by gas chromatography with ion-trap detection.
J Chromatogr. 1992 Mar 20 ;595(1-2):259-67.

PubMed
Construction of bacterial artificial chromosome library from electrochemical mic...
Construction of bacterial artificial chromosome library from electrochemical microorganisms.
FEMS Microbiol Lett. 2004 Sep 1 ;238(1):65-70.

PubMed
Purification and characterization of a cytosolic insulin-stimulated serine kinas...
Purification and characterization of a cytosolic insulin-stimulated serine kinase from rat liver.
J Biol Chem. 1992 May 15 ;267(14):9749-56.

PubMed
No evidence for sex differences in the severity and treatment of cancer pain.
No evidence for sex differences in the severity and treatment of cancer pain.
J Pain Symptom Manage. 2004 Sep ;28(3):225-32.

PubMed
Analysis of the glycosylation and phosphorylation of the alpha-subunit of the ly...
Analysis of the glycosylation and phosphorylation of the alpha-subunit of the lysosomal enzyme, beta-hexosaminidase A, by site-directed mutagenesis.
J Biol Chem. 1992 May 15 ;267(14):10039-44.

PubMed

Your browsing activity is empty.

Activity recording is turned off.

Turn recording back on

PubMed

Result Filters

Display Settings:

Send to: