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    Org Lett. 2002 Nov 28;4(24):4205-8.

    Preparation of C8-amine and acetylamine adducts of 2'-deoxyguanosine suitably protected for DNA synthesis.

    Gillet LC, Schärer OD.

    Institute of Medical Radiobiology, University of Zürich, August Forel Str. 7, 8008 Zürich, Switzerland.

    [reaction: see text] C8-Amine and acetylamine adducts of 2'-deoxyguanosine were synthesized. Our approach provides solutions for the coupling of aromatic amines to a protected 8-bromo-2'-deoxyguanosine derivative, for the selective acetylation of the coupled adduct at N(8) and for a protecting group scheme preserving the integrity of the base-labile N(8) acetyl group during DNA synthesis.

    PMID: 12443059 [PubMed - indexed for MEDLINE]

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