Crystal structure of methyl 1,2,3,4-tetra-O-acetyl...[Carbohydr Res. 2002]

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1: Carbohydr Res. 2002 Nov 19;337(21-23):2343-6. Links

Crystal structure of methyl 1,2,3,4-tetra-O-acetyl-beta-D-glucopyranuronate.

Root YY, Wagner TR, Norris P.

Department of Chemistry, Youngstown State University, 1 University Plaza, Youngstown, OH 44555-3663, USA.

The identity of the crystalline product formed by the acetylation of a mixture of methyl alpha- and beta-D-glucopyranuronates has been confirmed as being methyl 1,2,3,4-tetra-O-acetyl-beta-D-glucopyranuronate (3), which agrees with the assignment from 1H NMR. The absolute configuration of compound 3 was assigned to agree with the known chirality of the precursor sugar, D-glucono-6,3-lactone. Copyright 2002 Elsevier Science Ltd.

PMID: 12433499 [PubMed - indexed for MEDLINE]

Conformations of methyl 2,5-di-O-acetyl-beta-D-glucofuranosidurono-6,3-lactone and 1,2,5-tri-O-acetyl-beta-D-glucofuranurono-6,3-lactone in the crystal structure and in solution.
Carbohydr Res. 2006 Sep 25; 341(13):2275-85. Epub 2006 Jul 12.

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[Carbohydr Res. 2005]
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