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J Org Chem. 2002 May 3;67(9):3149-51.

Trimethylsilylethynyl ketones as surrogates for ethynyl ketones in the double Michael reaction.

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  • 1Department of Chemistry, University of Kentucky, Lexington, Kentucky 40506-0055, USA.

Abstract

Trimethylsilylethynyl ketones can be desilylated in the presence of a tethered carbon diacid and induced to undergo a double Michael reaction in situ. The trimethylsilylethynyl ketones can serve as surrogates of ethynyl ketones that are difficult to prepare or isolate.

PMID:
11975585
[PubMed - indexed for MEDLINE]
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