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    Forensic Sci Int. 2000 Mar 27;109(2):87-103.

    Study of the reaction mechanism of 1,8-diazafluoren-9-one with the amino acid, L-alanine.

    Wilkinson D.

    Source

    Forensic Identification Research Section, NPS Building, Room 503, Royal Canadian Mounted Police, 1200 Vanier Parkway, Ottawa, Ontario, Canada.

    Abstract

    This paper describes the study of the reaction between 1, 8-diazafluoren-9-one (DFO) with the amino acid L-alanine in methyl alcohol. Particular interest was paid to the possible role of the solvent which appears to react with the DFO to form a hemiketal that is the reactive species. A potential reaction pathway is proposed based on the current data collected. The reaction intermediates and products were identified by a variety of spectroscopic methods including mass spectrometry (MS), nuclear magnetic resonance (NMR) spectroscopy, and X-ray crystallography.

    PMID:
    10704813
    [PubMed - indexed for MEDLINE]

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